((S)-1-benzylpyrrolidin-2-yl)diphenylazidomethane

Base Information

Chemical Name:((S)-1-benzylpyrrolidin-2-yl)diphenylazidomethane
CAS No.:1072028-47-7
Molecular Formula:C₂₄H₂₄N₄
Molecular Weight:368.481
Hs Code.:

Synonyms:((S)-1-benzylpyrrolidin-2-yl)diphenylazidomethane

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Chemical Property of ((S)-1-benzylpyrrolidin-2-yl)diphenylazidomethane

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Technology Process of ((S)-1-benzylpyrrolidin-2-yl)diphenylazidomethane

There total 3 articles about ((S)-1-benzylpyrrolidin-2-yl)diphenylazidomethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 118970-95-9
(S)-1-benzyl-2-(hydroxydiphenylmethyl)pyrrolidine

: 1072028-47-7
((S)-1-benzylpyrrolidin-2-yl)diphenylazidomethane

Guidance literature:: With sodium azide; sulfuric acid; In chloroform; water; at 10 ℃; for 15h;
DOI:10.1016/j.tet.2015.11.032

Reference yield:

: 113304-84-0,127986-89-4
N-benzyl-(S)-proline methyl ester

: 1072028-47-7
((S)-1-benzylpyrrolidin-2-yl)diphenylazidomethane

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 12 h / 20 °C

2: sulfuric acid; trifluoroacetic acid; sodium azide; water / 6 h / 0 °C / Reflux

With sodium azide; sulfuric acid; water; trifluoroacetic acid; In tetrahydrofuran;
DOI:10.1016/j.tet.2012.12.024

Reference yield:

: 100-39-0
benzyl bromide

: 1072028-47-7
((S)-1-benzylpyrrolidin-2-yl)diphenylazidomethane

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane

1.2: 8 h / 25 °C

2.1: diethyl ether / 0 - 25 °C

3.1: sulfuric acid; sodium azide / chloroform / 0 - 25 °C

With sodium azide; sulfuric acid; In diethyl ether; dichloromethane; chloroform;
DOI:10.1021/acs.joc.9b03227