Technology Process of C28H39N3O3S
There total 8 articles about C28H39N3O3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
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Multi-step reaction with 2 steps
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / N,N-dimethyl-formamide
2: tetraphosphorus decasulfide / tetrahydrofuran
With
tetraphosphorus decasulfide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.12.116
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium hydride / N,N-dimethyl-formamide
2: trifluoroacetic acid; methoxybenzene / dichloromethane
3: potassium carbonate / dimethyl sulfoxide
4: hydrazine hydrate / tetrahydrofuran; ethanol
5: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / N,N-dimethyl-formamide
6: tetraphosphorus decasulfide / tetrahydrofuran
With
tetraphosphorus decasulfide; sodium hydride; potassium carbonate; benzotriazol-1-ol; hydrazine hydrate; methoxybenzene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid;
In
tetrahydrofuran; ethanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.12.116