8-(2-chlorophenyl)-8,13-dihydro-7H-benzo[b]naphtho-[1,2-e][1,4]diazepin-7-one

Base Information

Chemical Name:8-(2-chlorophenyl)-8,13-dihydro-7H-benzo[b]naphtho-[1,2-e][1,4]diazepin-7-one
CAS No.:1628347-75-0
Molecular Formula:C₂₃H₁₅ClN₂O
Molecular Weight:370.838
Hs Code.:

Synonyms:8-(2-chlorophenyl)-8,13-dihydro-7H-benzo[b]naphtho-[1,2-e][1,4]diazepin-7-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-(2-chlorophenyl)-8,13-dihydro-7H-benzo[b]naphtho-[1,2-e][1,4]diazepin-7-one

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Technology Process of 8-(2-chlorophenyl)-8,13-dihydro-7H-benzo[b]naphtho-[1,2-e][1,4]diazepin-7-one

There total 3 articles about 8-(2-chlorophenyl)-8,13-dihydro-7H-benzo[b]naphtho-[1,2-e][1,4]diazepin-7-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 615-43-0
2-iodophenylamine

: 1628347-91-0
C₁₇H₁₁ClINO

: 1628347-75-0
8-(2-chlorophenyl)-8,13-dihydro-7H-benzo[b]naphtho-[1,2-e][1,4]diazepin-7-one

Guidance literature:: With copper(l) iodide; potassium carbonate; In dimethyl sulfoxide; at 135 ℃; for 13h; Inert atmosphere;
DOI:10.1002/adsc.201301020

Reference yield:

: 91059-43-7
1-Iodo-2-naphthoic acid

: 1628347-75-0
8-(2-chlorophenyl)-8,13-dihydro-7H-benzo[b]naphtho-[1,2-e][1,4]diazepin-7-one

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / N,N-dimethyl-formamide / 3 h / 80 °C

2: pyridine / dichloromethane / 0 - 20 °C

3: potassium carbonate; copper(l) iodide / dimethyl sulfoxide / 13 h / 135 °C / Inert atmosphere

With pyridine; copper(l) iodide; thionyl chloride; potassium carbonate; In dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1002/adsc.201301020

Reference yield:

: 1261657-85-5
C₁₁H₆ClIO

: 95-51-2
o-chloroaniline

: 1628347-75-0
8-(2-chlorophenyl)-8,13-dihydro-7H-benzo[b]naphtho-[1,2-e][1,4]diazepin-7-one

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 0 - 20 °C

2: potassium carbonate; copper(l) iodide / dimethyl sulfoxide / 13 h / 135 °C / Inert atmosphere

With pyridine; copper(l) iodide; potassium carbonate; In dichloromethane; dimethyl sulfoxide;
DOI:10.1002/adsc.201301020