C₂₉H₂₀ClF₅N₂O₅

Base Information

Chemical Name:C₂₉H₂₀ClF₅N₂O₅
CAS No.:1192316-70-3
Molecular Formula:C₂₉H₂₀ClF₅N₂O₅
Molecular Weight:606.933
Hs Code.:

C<sub>29</sub>H<sub>20</sub>ClF<sub>5</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₂₉H₂₀ClF₅N₂O₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₂₀ClF₅N₂O₅

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Technology Process of C₂₉H₂₀ClF₅N₂O₅

There total 10 articles about C₂₉H₂₀ClF₅N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 454-78-4
3-bromo-4-chlorobenzotrifluoride

: C₂₂H₁₈F₂N₂O₅

: 1192316-70-3
C₂₉H₂₀ClF₅N₂O₅

Guidance literature:: With caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate; In toluene; at 20 - 100 ℃; for 21h;

Reference yield:

: 393-85-1
methyl 5-fluoro-2-nitrobenzoate

: 1192316-70-3
C₂₉H₂₀ClF₅N₂O₅

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate / 18-crown-6 ether / DMF (N,N-dimethylformamide) / 4 h / 20 °C

2: methanol / 1 h / 20 °C

3: pyridine / dichloromethane

4: caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / palladium diacetate / toluene / 19 h / 20 - 100 °C

5: hydrogen / palladium 10% on activated carbon / ethanol; ethyl acetate / 0.67 h / 20 °C / 760.05 Torr

6: caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / palladium diacetate / toluene / 21 h / 20 - 100 °C

With pyridine; hydrogen; potassium carbonate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; 18-crown-6 ether; palladium 10% on activated carbon; palladium diacetate; In methanol; DMF (N,N-dimethylformamide); ethanol; dichloromethane; ethyl acetate; toluene;

Reference yield:

: 320-98-9
5-fluoro-2-nitrobenzoic acid

: 1192316-70-3
C₂₉H₂₀ClF₅N₂O₅

Guidance literature:: Multi-step reaction with 7 steps

1: potassium carbonate / acetone / 50 h / 20 °C / Reflux

2: potassium carbonate / 18-crown-6 ether / DMF (N,N-dimethylformamide) / 4 h / 20 °C

3: methanol / 1 h / 20 °C

4: pyridine / dichloromethane

5: caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / palladium diacetate / toluene / 19 h / 20 - 100 °C

6: hydrogen / palladium 10% on activated carbon / ethanol; ethyl acetate / 0.67 h / 20 °C / 760.05 Torr

7: caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / palladium diacetate / toluene / 21 h / 20 - 100 °C

With pyridine; hydrogen; potassium carbonate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; 18-crown-6 ether; palladium 10% on activated carbon; palladium diacetate; In methanol; DMF (N,N-dimethylformamide); ethanol; dichloromethane; ethyl acetate; acetone; toluene;