dibutyl-[3-(4-triisopropylsilanyl-buta-1,3-diynyl)-phenyl]-amine

Base Information

Chemical Name:dibutyl-[3-(4-triisopropylsilanyl-buta-1,3-diynyl)-phenyl]-amine
CAS No.:367251-07-8
Molecular Formula:C₂₇H₄₃NSi
Molecular Weight:409.731
Hs Code.:

Synonyms:dibutyl-[3-(4-triisopropylsilanyl-buta-1,3-diynyl)-phenyl]-amine

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Chemical Property of dibutyl-[3-(4-triisopropylsilanyl-buta-1,3-diynyl)-phenyl]-amine

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Technology Process of dibutyl-[3-(4-triisopropylsilanyl-buta-1,3-diynyl)-phenyl]-amine

There total 1 articles about dibutyl-[3-(4-triisopropylsilanyl-buta-1,3-diynyl)-phenyl]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 149776-77-2
(Z)-(4-chlorobut-3-en-1-ynyl)triisopropylsilane

: 248276-92-8
N,N-dibutyl-3-iodoaniline

: 367251-07-8
dibutyl-[3-(4-triisopropylsilanyl-buta-1,3-diynyl)-phenyl]-amine

Guidance literature:: (Z)-(4-chlorobut-3-en-1-ynyl)triisopropylsilane; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.0833333h;

With zinc dibromide; In tetrahydrofuran; at -78 - 0 ℃; for 0.333333h;

N,N-dibutyl-3-iodoaniline; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; for 18h; Further stages.; Heating;
DOI:10.1021/ol016414u

Reference yield: 82.0%

: 367251-07-8
dibutyl-[3-(4-triisopropylsilanyl-buta-1,3-diynyl)-phenyl]-amine

: 1,8-di-(m-dibutylaminophenyl)-octa-1,3,5,7-tetrayne

Guidance literature:: With pyridine; copper diacetate; tetrabutyl ammonium fluoride; In tetrahydrofuran; diethyl ether; at 22 ℃; for 2h;
DOI:10.1021/ol016414u

Reference yield: 75.0%

: 367251-07-8
dibutyl-[3-(4-triisopropylsilanyl-buta-1,3-diynyl)-phenyl]-amine

: 367251-19-2
dibutyl-[4-iodo-3-(4-triisopropylsilanyl-buta-1,3-diynyl)-phenyl]-amine

Guidance literature:: With N,N,N-trimethylbenzenemethanaminium dichloroiodate; calcium carbonate; In methanol; dichloromethane; at 22 ℃; for 3h;
DOI:10.1021/ol016414u