benzyl 2-((S)-1-(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)-1-oxo-3-phenylpropan-2-yl)hydrazinecarboxylate

Base Information

Chemical Name:benzyl 2-((S)-1-(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)-1-oxo-3-phenylpropan-2-yl)hydrazinecarboxylate
CAS No.:1447498-19-2
Molecular Formula:C₂₇H₃₆N₂O₄
Molecular Weight:452.594
Hs Code.:

Synonyms:benzyl 2-((S)-1-(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)-1-oxo-3-phenylpropan-2-yl)hydrazinecarboxylate

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Chemical Property of benzyl 2-((S)-1-(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)-1-oxo-3-phenylpropan-2-yl)hydrazinecarboxylate

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Technology Process of benzyl 2-((S)-1-(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)-1-oxo-3-phenylpropan-2-yl)hydrazinecarboxylate

There total 5 articles about benzyl 2-((S)-1-(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)-1-oxo-3-phenylpropan-2-yl)hydrazinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 2216-51-5
(-)-menthol

: C₂₃H₂₁N₅O₃

: 1447498-19-2
benzyl 2-((S)-1-(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)-1-oxo-3-phenylpropan-2-yl)hydrazinecarboxylate

Guidance literature:: With dmap; In tetrahydrofuran; at 60 ℃; for 1h; Microwave irradiation;
DOI:10.1002/ejoc.201201731

Reference yield:

: 154006-07-2
(S)-2-(2-((benzyloxy)carbonyl)hydrazinyl)-3-phenylpropanoic acid

: 1447498-19-2
benzyl 2-((S)-1-(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)-1-oxo-3-phenylpropan-2-yl)hydrazinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / dichloromethane / 4 h / -10 °C

2: dmap / tetrahydrofuran / 1 h / 60 °C / Microwave irradiation

With dmap; thionyl chloride; In tetrahydrofuran; dichloromethane;
DOI:10.1002/ejoc.201201731

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 1447498-19-2
benzyl 2-((S)-1-(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)-1-oxo-3-phenylpropan-2-yl)hydrazinecarboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: potassium bromide; sodium nitrite; sulfuric acid / 6 h / -10 °C

2: hydrazine hydrate / ethanol / 70 °C / Microwave irradiation

3: triethylamine / water; acetonitrile / 20 °C

4: thionyl chloride / dichloromethane / 4 h / -10 °C

5: dmap / tetrahydrofuran / 1 h / 60 °C / Microwave irradiation

With dmap; thionyl chloride; sulfuric acid; hydrazine hydrate; triethylamine; potassium bromide; sodium nitrite; In tetrahydrofuran; ethanol; dichloromethane; water; acetonitrile;
DOI:10.1002/ejoc.201201731