2-Benzyl-6-(2-hydroxyethyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indol-1-on

Base Information

• Chemical Name: 2-Benzyl-6-(2-hydroxyethyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indol-1-on
• CAS No.: 162272-87-9
• Molecular Formula: C₂₀H₂₀N₂O₂
• Molecular Weight: 320.391

Synonyms:2-Benzyl-6-(2-hydroxyethyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indol-1-on

Chemical Property of 2-Benzyl-6-(2-hydroxyethyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indol-1-on

Chemical Property:

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Technology Process of 2-Benzyl-6-(2-hydroxyethyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indol-1-on

There total 2 articles about 2-Benzyl-6-(2-hydroxyethyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indol-1-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

6-(2-Ethanoyloxyethyl)-4,9-dihydro-pyrano<3,4-b>indol-1(3H)-on + benzylamine (100-46-9) → 2-Benzyl-6-(2-hydroxyethyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indol-1-on (162272-87-9)

Guidance literature:

at 200 - 240 ℃; for 14h;

DOI:10.1002/ardp.19943271107

Reference yield:

3-<4-(2-Hydroxyethyl)-phenylhydrazono>-5,6-dihydro-pyran-2(4H)-on (162272-77-7) → 2-Benzyl-6-(2-hydroxyethyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indol-1-on (162272-87-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / 1.25percent HCl / 0.17 h / Heating

2: 45 percent / 14 h / 200 - 240 °C

With hydrogenchloride;

DOI:10.1002/ardp.19943271107

Reference yield: 82.0%

2-Benzyl-6-(2-hydroxyethyl)-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indol-1-on (162272-87-9) → 2-(2-Benzyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indol-6-yl)-ethanol (162272-93-7)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; 1.) r.t., 1 h, 2.) reflux, 3 h;

DOI:10.1002/ardp.19943271107

upstream raw materials:

benzylamine

3-<4-(2-Hydroxyethyl)-phenylhydrazono>-5,6-dihydro-pyran-2(4H)-on

Downstream raw materials:

2-(2-Benzyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indol-6-yl)-ethanol

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