{(2S,5R)-2,6-Bis-benzyloxycarbonylamino-5-[(2R,3R,4S,5R,6R)-4,5-dihydroxy-6-hydroxymethyl-3-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-hexanoylamino}-acetic acid

Base Information

• Chemical Name: {(2S,5R)-2,6-Bis-benzyloxycarbonylamino-5-[(2R,3R,4S,5R,6R)-4,5-dihydroxy-6-hydroxymethyl-3-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-hexanoylamino}-acetic acid
• CAS No.: 75477-74-6
• Molecular Formula: C₆₄H₇₃N₃O₁₈
• Molecular Weight: 1172.29

Synonyms:{(2S,5R)-2,6-Bis-benzyloxycarbonylamino-5-[(2R,3R,4S,5R,6R)-4,5-dihydroxy-6-hydroxymethyl-3-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-hexanoylamino}-acetic acid

Chemical Property of {(2S,5R)-2,6-Bis-benzyloxycarbonylamino-5-[(2R,3R,4S,5R,6R)-4,5-dihydroxy-6-hydroxymethyl-3-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-hexanoylamino}-acetic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of {(2S,5R)-2,6-Bis-benzyloxycarbonylamino-5-[(2R,3R,4S,5R,6R)-4,5-dihydroxy-6-hydroxymethyl-3-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-hexanoylamino}-acetic acid

There total 31 articles about {(2S,5R)-2,6-Bis-benzyloxycarbonylamino-5-[(2R,3R,4S,5R,6R)-4,5-dihydroxy-6-hydroxymethyl-3-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-hexanoylamino}-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

{(2S,5R)-2,6-Bis-benzyloxycarbonylamino-5-[(2R,3R,4S,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-3-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-hexanoylamino}-acetic acid (75466-99-8) → {(2S,5R)-2,6-Bis-benzyloxycarbonylamino-5-[(2R,3R,4S,5R,6R)-4,5-dihydroxy-6-hydroxymethyl-3-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-hexanoylamino}-acetic acid (75477-74-6)

Guidance literature:

With water; triethylamine; In methanol; water; at 0 - 5 ℃; for 18h;

DOI:10.1016/S0040-4020(01)98942-2

Reference yield:

{(2R,5S)-2,6-Bis-benzyloxycarbonylamino-5-[(2S,3S,4R,5R,6S)-4,5-diacetoxy-6-acetoxymethyl-3-((2S,3S,4R,5S,6S)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-hexanoylamino}-acetic acid (75466-99-8) → {(2S,5R)-2,6-Bis-benzyloxycarbonylamino-5-[(2R,3R,4S,5R,6R)-4,5-dihydroxy-6-hydroxymethyl-3-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-hexanoylamino}-acetic acid (75477-74-6)

Guidance literature:

With water; triethylamine; In methanol; at 0 - 5 ℃; for 18h;

DOI:10.1016/S0040-4020(01)98942-2

Reference yield:

{(2R,5R)-2,6-Bis-benzyloxycarbonylamino-5-[(2S,3S,4R,5R,6S)-4,5-diacetoxy-6-acetoxymethyl-3-((2S,3S,4R,5S,6S)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-hexanoylamino}-acetic acid (75466-99-8) → {(2S,5S)-2,6-Bis-benzyloxycarbonylamino-5-[(2R,3R,4S,5R,6R)-4,5-dihydroxy-6-hydroxymethyl-3-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-hexanoylamino}-acetic acid (75477-74-6)

Guidance literature:

With water; triethylamine; In methanol; at 0 - 5 ℃; for 18h;

DOI:10.1016/S0040-4020(01)98942-2

upstream raw materials:

{(S)-2,6-Bis-benzyloxycarbonylamino-5-[(2R,3R,4S,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-3-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-hexanoylamino}-acetic acid

{(S)-2,6-Bis-benzyloxycarbonylamino-5-[(2R,3R,4S,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-3-((2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-hexanoylamino}-acetic acid tert-butyl ester

((S)-2,6-Bis-benzyloxycarbonylamino-5-hydroxy-hexanoylamino)-acetic acid tert-butyl ester

[(S)-2,6-Bis-benzyloxycarbonylamino-5-((2R,3R,4R,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-3-hydroxy-tetrahydro-pyran-2-yloxy)-hexanoylamino]-acetic acid tert-butyl ester

Downstream raw materials:

C₈₇H₁₁₂N₆O₂₅

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