dicarbobenzy-δ-hydroxy-L-lysyl-O-t-butylglycyl-O-3,4,6-tri-O-acetyl-β-D-galactopyranoside

Base Information

Chemical Name:dicarbobenzy-δ-hydroxy-L-lysyl-O-t-butylglycyl-O-3,4,6-tri-O-acetyl-β-D-galactopyranoside
CAS No.:75466-97-6
Molecular Formula:C₄₀H₅₃N₃O₁₆
Molecular Weight:831.871
Hs Code.:

Synonyms:dicarbobenzy-δ-hydroxy-L-lysyl-O-t-butylglycyl-O-3,4,6-tri-O-acetyl-β-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dicarbobenzy-δ-hydroxy-L-lysyl-O-t-butylglycyl-O-3,4,6-tri-O-acetyl-β-D-galactopyranoside

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Technology Process of dicarbobenzy-δ-hydroxy-L-lysyl-O-t-butylglycyl-O-3,4,6-tri-O-acetyl-β-D-galactopyranoside

There total 22 articles about dicarbobenzy-δ-hydroxy-L-lysyl-O-t-butylglycyl-O-3,4,6-tri-O-acetyl-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 75466-96-5
4-Oxo-pentanoic acid (2R,3R,4S,5S,6R)-4,5-diacetoxy-6-acetoxymethyl-2-[(1R,4S)-4-benzyloxycarbonylamino-1-(benzyloxycarbonylamino-methyl)-4-(tert-butoxycarbonylmethyl-carbamoyl)-butoxy]-tetrahydro-pyran-3-yl ester

: 75466-97-6
dicarbobenzy-δ-hydroxy-L-lysyl-O-t-butylglycyl-O-3,4,6-tri-O-acetyl-β-D-galactopyranoside

Guidance literature:: With hydrazine hydrate; acetylacetone; In pyridine; acetic acid; at 20 ℃; for 0.166667h;
DOI:10.1016/S0040-4020(01)98942-2

Reference yield:

: 75466-96-5
4-Oxo-pentanoic acid (2S,3S,4R,5R,6S)-4,5-diacetoxy-6-acetoxymethyl-2-[(1S,4R)-4-benzyloxycarbonylamino-1-(benzyloxycarbonylamino-methyl)-4-(tert-butoxycarbonylmethyl-carbamoyl)-butoxy]-tetrahydro-pyran-3-yl ester

: 75466-97-6
[(2R,5S)-2,6-Bis-benzyloxycarbonylamino-5-((2S,3S,4S,5R,6S)-4,5-diacetoxy-6-acetoxymethyl-3-hydroxy-tetrahydro-pyran-2-yloxy)-hexanoylamino]-acetic acid tert-butyl ester

Guidance literature:: With hydrazine hydrate; acetylacetone; In pyridine; acetic acid; at 20 ℃; for 0.166667h;
DOI:10.1016/S0040-4020(01)98942-2

Reference yield:

: 75466-96-5
4-Oxo-pentanoic acid (2S,3S,4R,5R,6S)-4,5-diacetoxy-6-acetoxymethyl-2-[(1R,4R)-4-benzyloxycarbonylamino-1-(benzyloxycarbonylamino-methyl)-4-(tert-butoxycarbonylmethyl-carbamoyl)-butoxy]-tetrahydro-pyran-3-yl ester

: 75466-97-6
[(2R,5R)-2,6-Bis-benzyloxycarbonylamino-5-((2S,3S,4S,5R,6S)-4,5-diacetoxy-6-acetoxymethyl-3-hydroxy-tetrahydro-pyran-2-yloxy)-hexanoylamino]-acetic acid tert-butyl ester

Guidance literature:: With hydrazine hydrate; acetylacetone; In pyridine; acetic acid; at 20 ℃; for 0.166667h;
DOI:10.1016/S0040-4020(01)98942-2