(1R,2S)-1-{[4-(methyloxy)phenyl]carbonyl}-2-phenylcyclopropanecarbonitrile

Base Information

Chemical Name:(1R,2S)-1-{[4-(methyloxy)phenyl]carbonyl}-2-phenylcyclopropanecarbonitrile
CAS No.:1309588-31-5
Molecular Formula:C₁₈H₁₅NO₂
Molecular Weight:277.323
Hs Code.:

Synonyms:(1R,2S)-1-{[4-(methyloxy)phenyl]carbonyl}-2-phenylcyclopropanecarbonitrile

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Chemical Property of (1R,2S)-1-{[4-(methyloxy)phenyl]carbonyl}-2-phenylcyclopropanecarbonitrile

Chemical Property:

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Technology Process of (1R,2S)-1-{[4-(methyloxy)phenyl]carbonyl}-2-phenylcyclopropanecarbonitrile

There total 2 articles about (1R,2S)-1-{[4-(methyloxy)phenyl]carbonyl}-2-phenylcyclopropanecarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 126893-72-9
2-(4-methoxyphenyl)-2-oxoethanecarbonimidoyl cyanide

: (1S,2R)-1-{[4-(methyloxy)phenyl]carbonyl}-2-phenylcyclopropanecarbonitrile

: 1309588-31-5
(1R,2S)-1-{[4-(methyloxy)phenyl]carbonyl}-2-phenylcyclopropanecarbonitrile

Guidance literature:: With tetrakis[(S)-(N-tetrachlorophthalimido)-tert-lucinato]dirhodium(II); In diethyl ether; at -35 ℃; for 16h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja201237j

Reference yield:

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 126893-72-9
2-(4-methoxyphenyl)-2-oxoethanecarbonimidoyl cyanide

: (1S,2R)-1-{[4-(methyloxy)phenyl]carbonyl}-2-phenylcyclopropanecarbonitrile

: 1309588-31-5
(1R,2S)-1-{[4-(methyloxy)phenyl]carbonyl}-2-phenylcyclopropanecarbonitrile

: (1RS,2RS)-1-{[4-(methyloxy)phenyl]carbonyl}-2-phenylcyclopropanecarbonitrile

Guidance literature:: With tetrakis[μ-(αS)-α-(1,1-dimethylethyl)-2,3-dihydro-1H-naphtho[1,8-cd]pyridine-2-acetato-κO:.kappaO']dirhodium(II)(Rh-Rh); In diethyl ether; at -35 ℃; for 16h; optical yield given as %ee; Inert atmosphere;
DOI:10.1021/ja201237j

Reference yield: 89.0%

: 1309588-31-5
(1R,2S)-1-{[4-(methyloxy)phenyl]carbonyl}-2-phenylcyclopropanecarbonitrile

: 1309588-50-8
4-(methyloxy)phenyl (1R,2S)-1-cyano-2-phenylcyclopropanecarboxylate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; isopropyl alcohol; at 65 - 70 ℃; for 5h; pH=7.5; regioselective reaction; aq. phosphate buffer;
DOI:10.1021/ja201237j