2-(4-methoxyphenyl)-2-oxoethanecarbonimidoyl cyanide

Base Information

Chemical Name:2-(4-methoxyphenyl)-2-oxoethanecarbonimidoyl cyanide
CAS No.:126893-72-9
Molecular Formula:C₁₀H₇N₃O₂
Molecular Weight:201.184
Hs Code.:

Synonyms:2-(4-methoxyphenyl)-2-oxoethanecarbonimidoyl cyanide

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Chemical Property of 2-(4-methoxyphenyl)-2-oxoethanecarbonimidoyl cyanide

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Technology Process of 2-(4-methoxyphenyl)-2-oxoethanecarbonimidoyl cyanide

There total 3 articles about 2-(4-methoxyphenyl)-2-oxoethanecarbonimidoyl cyanide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 13138-21-1
diazoacetonitrile

: 100-07-2
4-methoxy-benzoyl chloride

: 126893-72-9
2-(4-methoxyphenyl)-2-oxoethanecarbonimidoyl cyanide

Guidance literature:: With triethylamine; In chloroform; at -10 - 5 ℃; for 1h;

Reference yield: 85.0%

: 3672-47-7
3-oxo-3-(4'-methoxyphenyl)propanenitrile

: 126893-72-9
2-(4-methoxyphenyl)-2-oxoethanecarbonimidoyl cyanide

Guidance literature:: With pyridine; triflic azide; In hexane; acetonitrile; at 0 - 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ja201237j

Reference yield:

: 121-98-2
methyl 4-methoxybenzoate

: 126893-72-9
2-(4-methoxyphenyl)-2-oxoethanecarbonimidoyl cyanide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / Inert atmosphere; Reflux

2: triflic azide; pyridine / acetonitrile; hexane / 16 h / 0 - 20 °C / Inert atmosphere; Sealed tube

With pyridine; triflic azide; sodium hydride; In hexane; acetonitrile;
DOI:10.1002/anie.201707375