C₁₉H₁₉NO

Base Information

Chemical Name:C₁₉H₁₉NO
CAS No.:1620404-32-1
Molecular Formula:C₁₉H₁₉NO
Molecular Weight:277.366
Hs Code.:

Synonyms:C₁₉H₁₉NO

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Chemical Property of C₁₉H₁₉NO

Chemical Property:

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Technology Process of C₁₉H₁₉NO

There total 4 articles about C₁₉H₁₉NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1620404-09-2
C₁₉H₂₀N₂O₂

: 1620404-32-1
C₁₉H₁₉NO

Guidance literature:: With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; sodium acetate; In 1,2-dichloro-ethane; at 100 ℃; for 12h; Glovebox;
DOI:10.1021/ol501599j

Reference yield:

: 591-50-4
iodobenzene

: 1620404-32-1
C₁₉H₁₉NO

Guidance literature:: Multi-step reaction with 8 steps

1.1: piperidine; copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / toluene / 2 h / 20 °C

2.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

3.1: zinc; acetic acid / dichloromethane / 0 °C

4.1: triethylamine / tetrahydrofuran / 0 °C

5.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h

5.2: 20 °C

6.1: potassium hydroxide; water / Heating

7.1: sodium nitrite; acetic acid / water / 2 h / 0 °C

8.1: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; silver hexafluoroantimonate; sodium acetate / 1,2-dichloro-ethane / 12 h / 100 °C / Glovebox

With piperidine; bis-triphenylphosphine-palladium(II) chloride; silver hexafluoroantimonate; copper(l) iodide; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; di-isopropyl azodicarboxylate; water; sodium acetate; sodium hydride; acetic acid; triethylamine; triphenylphosphine; potassium hydroxide; zinc; sodium nitrite; In tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol501599j

Reference yield:

: 69936-53-4
6-phenylhex-5-yn-1-ol

: 1620404-32-1
C₁₉H₁₉NO

Guidance literature:: Multi-step reaction with 7 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

2.1: zinc; acetic acid / dichloromethane / 0 °C

3.1: triethylamine / tetrahydrofuran / 0 °C

4.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h

4.2: 20 °C

5.1: potassium hydroxide; water / Heating

6.1: sodium nitrite; acetic acid / water / 2 h / 0 °C

7.1: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; silver hexafluoroantimonate; sodium acetate / 1,2-dichloro-ethane / 12 h / 100 °C / Glovebox

With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; di-isopropyl azodicarboxylate; water; sodium acetate; sodium hydride; acetic acid; triethylamine; triphenylphosphine; potassium hydroxide; zinc; sodium nitrite; In tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1021/ol501599j