5-Hexyn-1-ol, 6-phenyl-

Base Information

Chemical Name:5-Hexyn-1-ol, 6-phenyl-
CAS No.:69936-53-4
Molecular Formula:C12H14O
Molecular Weight:174.243
Hs Code.:
DSSTox Substance ID:DTXSID20446360
Nikkaji Number:J756.901G
Wikidata:Q82264984

Synonyms:5-Hexyn-1-ol, 6-phenyl-;69936-53-4;6-phenylhex-5-yn-1-ol;6-Phenyl-5-hexyn-1-ol;SCHEMBL2947602;DTXSID20446360

Suppliers and Price of 5-Hexyn-1-ol, 6-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 5-Hexyn-1-ol, 6-phenyl-

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:174.104465066
Heavy Atom Count:13
Complexity:178

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C#CCCCCO

Technology Process of 5-Hexyn-1-ol, 6-phenyl-

There total 9 articles about 5-Hexyn-1-ol, 6-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 591-50-4
iodobenzene

: 928-90-5
5-hexyl-1-ol

: 69936-53-4
6-phenylhex-5-yn-1-ol

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/acs.orglett.6b02537

Reference yield: 96.0%

: 41049-30-3
2-(4-iodobutoxy)tetrahydropyran

: 536-74-3
phenylacetylene

: 69936-53-4
6-phenylhex-5-yn-1-ol

Guidance literature:: phenylacetylene; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 1.5h; Inert atmosphere;

2-(4-iodobutoxy)tetrahydropyran; With N,N,N,N,N,N-hexamethylphosphoric triamide; In tetrahydrofuran; hexane; at 0 - 20 ℃; for 12.5h; Inert atmosphere;

With toluene-4-sulfonic acid; In methanol; water; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1246/cl.2010.766