methyl 2-(m-methoxyphenyl)-1-methyl-1,2,3,6-tetrahydropyridine-4-acetate

Base Information

Chemical Name:methyl 2-(m-methoxyphenyl)-1-methyl-1,2,3,6-tetrahydropyridine-4-acetate
CAS No.:95533-14-5
Molecular Formula:C₁₆H₂₁NO₃
Molecular Weight:275.348
Hs Code.:

Synonyms:methyl 2-(m-methoxyphenyl)-1-methyl-1,2,3,6-tetrahydropyridine-4-acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-(m-methoxyphenyl)-1-methyl-1,2,3,6-tetrahydropyridine-4-acetate

Chemical Property:

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Technology Process of methyl 2-(m-methoxyphenyl)-1-methyl-1,2,3,6-tetrahydropyridine-4-acetate

There total 2 articles about methyl 2-(m-methoxyphenyl)-1-methyl-1,2,3,6-tetrahydropyridine-4-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.0%

: 36282-40-3
(3-methoxyphenyl)magnesium bromide

: 95533-10-1
methyl 2-cyano-1-methyl-1,2,3,6-tetrahydropyridine-4-acetate

: 95533-14-5
methyl 2-(m-methoxyphenyl)-1-methyl-1,2,3,6-tetrahydropyridine-4-acetate

: 95533-15-6
1,1-bis(m-methoxyphenyl)-2-<2-(m-methoxyphenyl)-1-methyl-1,2,3,6-tetrahydro-4-pyridyl>ethanol

Guidance literature:: In tetrahydrofuran; for 48h; Ambient temperature;
DOI:10.1021/jo00209a031

Reference yield:

: 39998-19-1
4-<(methoxycarbonyl)methyl>-1-methylpyridinium iodide

: 95533-14-5
methyl 2-(m-methoxyphenyl)-1-methyl-1,2,3,6-tetrahydropyridine-4-acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 6 N aq. HCl, 2.) NaBH₄ / 2.) Et₂O, RT, 4 h

2: 70 percent / tetrahydrofuran / 48 h / Ambient temperature

With hydrogenchloride; sodium tetrahydroborate; In tetrahydrofuran;
DOI:10.1021/jo00209a031

Reference yield:

: 95533-14-5
methyl 2-(m-methoxyphenyl)-1-methyl-1,2,3,6-tetrahydropyridine-4-acetate

: 95533-17-8
methyl 1-methyl-2-(m-methoxyphenyl)piperidine-4-acetate

: 95533-21-4
methyl 1-methyl-2-(m-methoxyphenyl)piperidine-4-acetate

Guidance literature:: With hydrogen; platinum(IV) oxide; In methanol; under 760 Torr; Yield given. Yields of byproduct given; Ambient temperature;
DOI:10.1021/jo00209a031