(S)-tert-butyl 2-(N-allyl-4-nitrophenylsulphonamido)-3-phenylpropanoate

Base Information

Chemical Name:(S)-tert-butyl 2-(N-allyl-4-nitrophenylsulphonamido)-3-phenylpropanoate
CAS No.:1190383-11-9
Molecular Formula:C₂₂H₂₆N₂O₆S
Molecular Weight:446.524
Hs Code.:

Synonyms:(S)-tert-butyl 2-(N-allyl-4-nitrophenylsulphonamido)-3-phenylpropanoate

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Chemical Property of (S)-tert-butyl 2-(N-allyl-4-nitrophenylsulphonamido)-3-phenylpropanoate

Chemical Property:

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Technology Process of (S)-tert-butyl 2-(N-allyl-4-nitrophenylsulphonamido)-3-phenylpropanoate

There total 3 articles about (S)-tert-butyl 2-(N-allyl-4-nitrophenylsulphonamido)-3-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 106-95-6
allyl bromide

: 221285-90-1
(S)-tert-butyl 2-(4-nitrophenylsulphonamido)-3-phenylpropanoate

: 1190383-11-9
(S)-tert-butyl 2-(N-allyl-4-nitrophenylsulphonamido)-3-phenylpropanoate

Guidance literature:: With N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate; In acetonitrile; at 25 ℃; for 13h;
DOI:10.1039/b910326k

Reference yield:

: 98-74-8
4-Nitrobenzenesulfonyl chloride

: 1190383-11-9
(S)-tert-butyl 2-(N-allyl-4-nitrophenylsulphonamido)-3-phenylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / 25 °C

1.2: 0 °C

2.1: potassium carbonate; N-benzyl-N,N,N-triethylammonium chloride / acetonitrile / 25 °C

With N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate; N-ethyl-N,N-diisopropylamine; In dichloromethane; acetonitrile;
DOI:10.1002/adsc.202100493

Reference yield:

: 15100-75-1,75898-47-4
L-phenylalanine tert-butyl ester hydrochloride

: 1190383-11-9
(S)-tert-butyl 2-(N-allyl-4-nitrophenylsulphonamido)-3-phenylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / 25 °C

1.2: 0 °C

2.1: potassium carbonate; N-benzyl-N,N,N-triethylammonium chloride / acetonitrile / 25 °C

With N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate; N-ethyl-N,N-diisopropylamine; In dichloromethane; acetonitrile;
DOI:10.1002/adsc.202100493