(3-{2-[(benzyl-methoxycarbonyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid

Base Information

Chemical Name:(3-{2-[(benzyl-methoxycarbonyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid
CAS No.:1198281-54-7
Molecular Formula:C₂₄H₂₂BrNO₅
Molecular Weight:484.346
Hs Code.:

Synonyms:(3-{2-[(benzyl-methoxycarbonyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid

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Chemical Property of (3-{2-[(benzyl-methoxycarbonyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid

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Technology Process of (3-{2-[(benzyl-methoxycarbonyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid

There total 4 articles about (3-{2-[(benzyl-methoxycarbonyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 42058-59-3
3-hydroxy-benzeneacetic acid, methyl ester

: 1198281-54-7
(3-{2-[(benzyl-methoxycarbonyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / 1,4-dioxane / 100 °C

2.1: sodium cyanoborohydride; acetic acid / dichloromethane / 20 °C

3.1: triethylamine / dichloromethane / 20 °C

4.1: water; lithium hydroxide / tetrahydrofuran / 20 °C

4.2: pH 3 - 4

With water; sodium cyanoborohydride; potassium carbonate; acetic acid; triethylamine; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; dichloromethane;

Reference yield:

: 1198281-56-9
(3-{2-[(benzyl-methoxycarbonyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid methyl ester

: 1198281-54-7
(3-{2-[(benzyl-methoxycarbonyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid

Guidance literature:: (3-{2-[(benzyl-methoxycarbonyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid methyl ester; With water; lithium hydroxide; In tetrahydrofuran; at 20 ℃;

With hydrogenchloride; In tetrahydrofuran; water; pH=3 - 4;

Reference yield:

: 621-37-4
m-hydroxyphenylacetic acid

: 1198281-54-7
(3-{2-[(benzyl-methoxycarbonyl-amino)-methyl]-4-bromo-phenoxy}-phenyl)-acetic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: thionyl chloride / 0.5 h

2.1: potassium carbonate / 1,4-dioxane / 100 °C

3.1: sodium cyanoborohydride; acetic acid / dichloromethane / 20 °C

4.1: triethylamine / dichloromethane / 20 °C

5.1: water; lithium hydroxide / tetrahydrofuran / 20 °C

5.2: pH 3 - 4

With thionyl chloride; water; sodium cyanoborohydride; potassium carbonate; acetic acid; triethylamine; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; dichloromethane;