7-chloro-3,4-dihydro-3-<4-(trifluoromethyl)phenyl>-1(2H)-acridinone 10-oxide

Base Information

Chemical Name:7-chloro-3,4-dihydro-3-<4-(trifluoromethyl)phenyl>-1(2H)-acridinone 10-oxide
CAS No.:144155-88-4
Molecular Formula:C₂₀H₁₃ClF₃NO₂
Molecular Weight:391.777
Hs Code.:

Synonyms:7-chloro-3,4-dihydro-3-<4-(trifluoromethyl)phenyl>-1(2H)-acridinone 10-oxide

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Chemical Property of 7-chloro-3,4-dihydro-3-<4-(trifluoromethyl)phenyl>-1(2H)-acridinone 10-oxide

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Technology Process of 7-chloro-3,4-dihydro-3-<4-(trifluoromethyl)phenyl>-1(2H)-acridinone 10-oxide

There total 7 articles about 7-chloro-3,4-dihydro-3-<4-(trifluoromethyl)phenyl>-1(2H)-acridinone 10-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 144155-69-1
7-chloro-3,4-dihydro-3-<4-(trifluoromethyl)phenyl>-1(2H)-acridinone

: 144155-88-4
7-chloro-3,4-dihydro-3-<4-(trifluoromethyl)phenyl>-1(2H)-acridinone 10-oxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform; Ambient temperature;
DOI:10.1021/jm00097a001

Reference yield:

: 455-19-6
4-Trifluoromethylbenzaldehyde

: 144155-88-4
7-chloro-3,4-dihydro-3-<4-(trifluoromethyl)phenyl>-1(2H)-acridinone 10-oxide

Guidance literature:: Multi-step reaction with 6 steps

1: 32 percent / 50percent aq. NaOH / 72 h / Ambient temperature

2: EtONa / ethanol / 6 h / Heating

3: 2 N NaOH / 2 h / Heating

4: 5 N H₂SO₄ / 4.5 h / Heating

5: 50 percent / piperidine / ethanol / Heating

6: 78 percent / 85percent m-chloroperoxybenzoic acid / CHCl₃ / Ambient temperature

With piperidine; sodium hydroxide; sulfuric acid; sodium ethanolate; 3-chloro-benzenecarboperoxoic acid; In ethanol; chloroform;
DOI:10.1021/jm00097a001

Reference yield:

: 20028-53-9
2-amino-5-chlorobenzaldehyde

: 144155-88-4
7-chloro-3,4-dihydro-3-<4-(trifluoromethyl)phenyl>-1(2H)-acridinone 10-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / piperidine / ethanol / Heating

2: 78 percent / 85percent m-chloroperoxybenzoic acid / CHCl₃ / Ambient temperature

With piperidine; 3-chloro-benzenecarboperoxoic acid; In ethanol; chloroform;
DOI:10.1021/jm00097a001