p-tolyl-6-O-[tert-butyl(diphenyl)silyl]-2,3,4-tri-O-benzyl-1-thio-β-D-galactopyranoside

Base Information

Chemical Name:p-tolyl-6-O-[tert-butyl(diphenyl)silyl]-2,3,4-tri-O-benzyl-1-thio-β-D-galactopyranoside
CAS No.:1030376-69-2
Molecular Formula:C₅₀H₅₄O₅SSi
Molecular Weight:795.127
Hs Code.:

Synonyms:p-tolyl-6-O-[tert-butyl(diphenyl)silyl]-2,3,4-tri-O-benzyl-1-thio-β-D-galactopyranoside

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Chemical Property of p-tolyl-6-O-[tert-butyl(diphenyl)silyl]-2,3,4-tri-O-benzyl-1-thio-β-D-galactopyranoside

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Technology Process of p-tolyl-6-O-[tert-butyl(diphenyl)silyl]-2,3,4-tri-O-benzyl-1-thio-β-D-galactopyranoside

There total 1 articles about p-tolyl-6-O-[tert-butyl(diphenyl)silyl]-2,3,4-tri-O-benzyl-1-thio-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 502763-89-5
4-methylphenyl 6-O-tert-butyldiphenylsilyl-1-thio-β-D-galactopyranoside

: 1030376-69-2
p-tolyl-6-O-[tert-butyl(diphenyl)silyl]-2,3,4-tri-O-benzyl-1-thio-β-D-galactopyranoside

Guidance literature:: 4-methylphenyl 6-O-tert-butyldiphenylsilyl-1-thio-β-D-galactopyranoside; With tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.25h;

benzyl bromide; In tetrahydrofuran; at 45 ℃; for 6h; Further stages.;
DOI:10.1016/j.tetlet.2008.03.032

Reference yield: 60.0%

: 1030376-69-2
p-tolyl-6-O-[tert-butyl(diphenyl)silyl]-2,3,4-tri-O-benzyl-1-thio-β-D-galactopyranoside

: 152840-34-1
1-deoxy-3,4,6-tri-O-benzyl-D-glucopyranose

: 1030376-70-5
C₇₀H₇₆O₁₀Si

: 1030376-71-6
C₇₀H₇₆O₁₀Si

Guidance literature:: With N-iodo-succinimide; molecular sieve; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 - 20 ℃;
DOI:10.1016/j.tetlet.2008.03.032