2-((S)-4-Benzyloxycarbonylamino-4-carboxy-butylcarbamoyl)-cyclopropanecarboxylic acid ethyl ester

Base Information

Chemical Name:2-((S)-4-Benzyloxycarbonylamino-4-carboxy-butylcarbamoyl)-cyclopropanecarboxylic acid ethyl ester
CAS No.:1055036-70-8
Molecular Formula:C₂₀H₂₆N₂O₇
Molecular Weight:406.436
Hs Code.:

Synonyms:2-((S)-4-Benzyloxycarbonylamino-4-carboxy-butylcarbamoyl)-cyclopropanecarboxylic acid ethyl ester

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Chemical Property of 2-((S)-4-Benzyloxycarbonylamino-4-carboxy-butylcarbamoyl)-cyclopropanecarboxylic acid ethyl ester

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Technology Process of 2-((S)-4-Benzyloxycarbonylamino-4-carboxy-butylcarbamoyl)-cyclopropanecarboxylic acid ethyl ester

There total 2 articles about 2-((S)-4-Benzyloxycarbonylamino-4-carboxy-butylcarbamoyl)-cyclopropanecarboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2640-58-6
Nα-benzyloxycarbonyl-L-ornithine

: 178687-20-2
2-chlorocarbonyl-cyclopropanecarboxylic acid ethyl ester

: 1055036-70-8
2-((S)-4-Benzyloxycarbonylamino-4-carboxy-butylcarbamoyl)-cyclopropanecarboxylic acid ethyl ester

Guidance literature:: With potassium carbonate; In dichloromethane; for 8h;
DOI:10.1248/cpb.45.1146

Reference yield:

: 167113-73-7
D,L-Trans-2-Ethoxycarbonylcyclopropane-1-carboxylic acid

: 1055036-70-8
2-((S)-4-Benzyloxycarbonylamino-4-carboxy-butylcarbamoyl)-cyclopropanecarboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / dimethylformamide / 1 h / Heating

2: K₂CO₃ / CH₂Cl₂ / 8 h

With thionyl chloride; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1248/cpb.45.1146

Reference yield:

: 1055036-70-8
2-((S)-4-Benzyloxycarbonylamino-4-carboxy-butylcarbamoyl)-cyclopropanecarboxylic acid ethyl ester

: 194206-09-2
methyl N^α-[(1-benzyloxycarbonylindolin-5-yl)carbonyl]-N^δ-[2-(ethoxycarbonyl)cyclopropylcarbonyl]-L-ornithinate

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 2 h / Heating

2: 76 percent / H₂ / 5percent Pd/C / methanol / 10 h

3: aq. K₂CO₃ / CH₂Cl₂ / 10 h / Ambient temperature

With thionyl chloride; hydrogen; potassium carbonate; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1248/cpb.45.1146