C₅₆H₅₆O₇S₂Si

Base Information

Chemical Name:C₅₆H₅₆O₇S₂Si
CAS No.:537658-29-0
Molecular Formula:C₅₆H₅₆O₇S₂Si
Molecular Weight:933.274
Hs Code.:

C<sub>56</sub>H<sub>56</sub>O<sub>7</sub>S<sub>2</sub>Si

Synonyms:C₅₆H₅₆O₇S₂Si

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Chemical Property of C₅₆H₅₆O₇S₂Si

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Technology Process of C₅₆H₅₆O₇S₂Si

There total 10 articles about C₅₆H₅₆O₇S₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: C₂₇H₂₉ClOS₂Si

: 537658-16-5
(2E,4E)-2-Benzyloxymethyl-hexa-2,4-dienedioic acid 1-((1S,2S)-2-hydroxy-1,2-diphenyl-ethyl) ester 6-methyl ester

: 537658-29-0
C₅₆H₅₆O₇S₂Si

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1021/ol034218c

Reference yield:

: 100-39-0
benzyl bromide

: 537658-29-0
C₅₆H₅₆O₇S₂Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: 78 percent / NaH; Bu₄NI / dimethylformamide / 1 h / 0 - 20 °C

2.1: 75 percent / n-BuLi / tetrahydrofuran; hexane / 0 - 20 °C

3.1: O₃ / CH₂Cl₂; methanol / 0.08 h / -78 °C

3.2: 75 percent / Me₂S / CH₂Cl₂; methanol / 14 h / -78 - 20 °C

4.1: 75 percent / MgBr₂; Et₃N / tetrahydrofuran / 2.5 h

5.1: 100 percent / HF / acetonitrile / 24 h / 20 °C

6.1: 63 percent / DMAP; Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

With dmap; n-butyllithium; hydrogen fluoride; tetra-(n-butyl)ammonium iodide; sodium hydride; ozone; triethylamine; magnesium bromide; In tetrahydrofuran; methanol; hexane; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 4.1: modified Horner-Wadsworth-Emmons reaction;
DOI:10.1021/ol034218c

Reference yield:

: 124957-46-6
(2E,4E)-methyl 2-acetoxymethyl-5-phenyl-penta-2,4-dienoate

: 537658-29-0
C₅₆H₅₆O₇S₂Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: 100 percent / K₂CO₃ / methanol / 4 h / 20 °C

2.1: 78 percent / NaH; Bu₄NI / dimethylformamide / 1 h / 0 - 20 °C

3.1: 75 percent / n-BuLi / tetrahydrofuran; hexane / 0 - 20 °C

4.1: O₃ / CH₂Cl₂; methanol / 0.08 h / -78 °C

4.2: 75 percent / Me₂S / CH₂Cl₂; methanol / 14 h / -78 - 20 °C

5.1: 75 percent / MgBr₂; Et₃N / tetrahydrofuran / 2.5 h

6.1: 100 percent / HF / acetonitrile / 24 h / 20 °C

7.1: 63 percent / DMAP; Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

With dmap; n-butyllithium; hydrogen fluoride; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; ozone; triethylamine; magnesium bromide; In tetrahydrofuran; methanol; hexane; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 5.1: modified Horner-Wadsworth-Emmons reaction;
DOI:10.1021/ol034218c