4-benzyl-5-(2-methoxyphenyl)-1-(4-methylphenylsulfonyl)-3-(4-nitrophenyl)-4,5-dihydro-1H-[1,2,4]triazole

Base Information

• Chemical Name: 4-benzyl-5-(2-methoxyphenyl)-1-(4-methylphenylsulfonyl)-3-(4-nitrophenyl)-4,5-dihydro-1H-[1,2,4]triazole
• CAS No.: 1224734-97-7
• Molecular Formula: C₂₉H₂₆N₄O₅S
• Molecular Weight: 542.615

Synonyms:4-benzyl-5-(2-methoxyphenyl)-1-(4-methylphenylsulfonyl)-3-(4-nitrophenyl)-4,5-dihydro-1H-[1,2,4]triazole

Chemical Property of 4-benzyl-5-(2-methoxyphenyl)-1-(4-methylphenylsulfonyl)-3-(4-nitrophenyl)-4,5-dihydro-1H-[1,2,4]triazole

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of 4-benzyl-5-(2-methoxyphenyl)-1-(4-methylphenylsulfonyl)-3-(4-nitrophenyl)-4,5-dihydro-1H-[1,2,4]triazole

There total 1 articles about 4-benzyl-5-(2-methoxyphenyl)-1-(4-methylphenylsulfonyl)-3-(4-nitrophenyl)-4,5-dihydro-1H-[1,2,4]triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

4-methyl-N'-[(4-nitrophenyl)methylidene]benzene-1-sulfonohydrazide (1747-50-8) + N‐benzyl‐1‐(2‐methoxyphenyl)methanimine → 4-benzyl-3-(2-methoxyphenyl)-5-(4-nitrophenyl)-4H-[1,2,4]triazole (1224734-98-8) + 4-benzyl-5-(2-methoxyphenyl)-1-(4-methylphenylsulfonyl)-3-(4-nitrophenyl)-4,5-dihydro-1H-[1,2,4]triazole (1224734-97-7)

Guidance literature:

With iodosylbenzene; magnesium sulfate; In dichloromethane; at 0 - 20 ℃; for 3h; regioselective reaction;

DOI:10.1039/b924761k

Reference yield: 95.0%

4-benzyl-5-(2-methoxyphenyl)-1-(4-methylphenylsulfonyl)-3-(4-nitrophenyl)-4,5-dihydro-1H-[1,2,4]triazole (1224734-97-7) → 4-benzyl-3-(2-methoxyphenyl)-5-(4-nitrophenyl)-4H-[1,2,4]triazole (1224734-98-8)

Guidance literature:

With N-Bromosuccinimide; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1039/b924761k

upstream raw materials:

4-methyl-N'-[(4-nitrophenyl)methylidene]benzene-1-sulfonohydrazide

Downstream raw materials:

4-benzyl-3-(2-methoxyphenyl)-5-(4-nitrophenyl)-4H-[1,2,4]triazole

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