4-Acetamino-2,5-dibutoxyanilin

Base Information

• Chemical Name: 4-Acetamino-2,5-dibutoxyanilin
• CAS No.: 77892-65-0
• Molecular Formula: C₁₆H₂₆N₂O₃
• Molecular Weight: 294.394
• Mol file: 77892-65-0.mol

Synonyms:4-Acetamino-2,5-dibutoxyanilin

Chemical Property of 4-Acetamino-2,5-dibutoxyanilin

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 4-Acetamino-2,5-dibutoxyanilin

There total 2 articles about 4-Acetamino-2,5-dibutoxyanilin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2,5-Dibutoxy-4-nitroacetanilid (77892-64-9) → 4-Acetamino-2,5-dibutoxyanilin (77892-65-0)

Guidance literature:

With hydrazine hydrate; nickel; In methanol; for 1h; Heating;

Reference yield:

2,5-dibutoxy-aniline (136-76-5) → 4-Acetamino-2,5-dibutoxyanilin (77892-65-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 2.) 6 N HNO₃ / 1.) glacial AcOH, reflux, 2.) 1 h, 10-15 deg C

2: 95 percent / 80percent hydrazine hydrate / Raney-Nickel / methanol / 1 h / Heating

With nitric acid; hydrazine hydrate; nickel; In methanol;

upstream raw materials:

2,5-Dibutoxy-4-nitroacetanilid

2,5-dibutoxy-aniline

Refernces