N-tert-butoxycarbonyl-2-{(4'-[1'',3'']-dithiolan-2''-yl)phenyl}pyrrole

Base Information

Chemical Name:N-tert-butoxycarbonyl-2-{(4'-[1'',3'']-dithiolan-2''-yl)phenyl}pyrrole
CAS No.:1008788-51-9
Molecular Formula:C₁₈H₂₁NO₂S₂
Molecular Weight:347.502
Hs Code.:

Synonyms:N-tert-butoxycarbonyl-2-{(4'-[1'',3'']-dithiolan-2''-yl)phenyl}pyrrole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-tert-butoxycarbonyl-2-{(4'-[1'',3'']-dithiolan-2''-yl)phenyl}pyrrole

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Technology Process of N-tert-butoxycarbonyl-2-{(4'-[1'',3'']-dithiolan-2''-yl)phenyl}pyrrole

There total 3 articles about N-tert-butoxycarbonyl-2-{(4'-[1'',3'']-dithiolan-2''-yl)phenyl}pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 1008788-49-5
2-(4-formyl-phenyl)-pyrrole-1-carboxylic acid tert-butyl ester

: 540-63-6
ethane-1,2-dithiol

: 1008788-51-9
N-tert-butoxycarbonyl-2-{(4'-[1'',3'']-dithiolan-2''-yl)phenyl}pyrrole

Guidance literature:: With kaolin; In benzene; for 18h; Heating;
DOI:10.1246/cl.2006.708

Reference yield:

: 4-formylphenylboronic acid disodium salt

: 1008788-51-9
N-tert-butoxycarbonyl-2-{(4'-[1'',3'']-dithiolan-2''-yl)phenyl}pyrrole

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / aq. Na₂CO₃ / Pd(PPh₃)4 / toluene; methanol / 16 h / 80 °C

2: 36 percent / kaolin / benzene / 18 h / Heating

With kaolin; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; toluene; benzene;
DOI:10.1246/cl.2006.708

Reference yield:

: 117657-37-1
2-bromo-pyrrole-1-carboxylic acid tert-butyl ester

: 1008788-51-9
N-tert-butoxycarbonyl-2-{(4'-[1'',3'']-dithiolan-2''-yl)phenyl}pyrrole

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / aq. Na₂CO₃ / Pd(PPh₃)4 / toluene; methanol / 16 h / 80 °C

2: 36 percent / kaolin / benzene / 18 h / Heating

With kaolin; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; toluene; benzene;
DOI:10.1246/cl.2006.708