N-But-2-ynyl-N-((S)-1-methoxymethoxymethyl-allyl)-4-methyl-benzenesulfonamide

Base Information

Chemical Name:N-But-2-ynyl-N-((S)-1-methoxymethoxymethyl-allyl)-4-methyl-benzenesulfonamide
CAS No.:150674-63-8
Molecular Formula:C₁₇H₂₃NO₄S
Molecular Weight:337.44
Hs Code.:

Synonyms:N-But-2-ynyl-N-((S)-1-methoxymethoxymethyl-allyl)-4-methyl-benzenesulfonamide

Suppliers and Price of N-But-2-ynyl-N-((S)-1-methoxymethoxymethyl-allyl)-4-methyl-benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-But-2-ynyl-N-((S)-1-methoxymethoxymethyl-allyl)-4-methyl-benzenesulfonamide

Chemical Property:

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Technology Process of N-But-2-ynyl-N-((S)-1-methoxymethoxymethyl-allyl)-4-methyl-benzenesulfonamide

There total 2 articles about N-But-2-ynyl-N-((S)-1-methoxymethoxymethyl-allyl)-4-methyl-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 61493-85-4
but-2-yn-1-yl methanesulfonate

: 150674-62-7
(S)-N-[1-(methoxy)methoxy-3-buten-2-yl]-4-methylbenzenesulfonamide

: 150674-63-8
N-But-2-ynyl-N-((S)-1-methoxymethoxymethyl-allyl)-4-methyl-benzenesulfonamide

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1016/S0040-4039(00)79176-3

Reference yield:

: 150674-61-6
((S)-1-Methoxymethoxymethyl-allyl)-carbamic acid benzyl ester

: 150674-63-8
N-But-2-ynyl-N-((S)-1-methoxymethoxymethyl-allyl)-4-methyl-benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1) Li, NH₃, 2) Na₂CO₃ / 1) THF, -33 deg C, 2) RT

2: 88 percent / NaH / dimethylformamide / Ambient temperature

With ammonia; lithium; sodium hydride; sodium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)79176-3

Reference yield:

: 150674-63-8
N-But-2-ynyl-N-((S)-1-methoxymethoxymethyl-allyl)-4-methyl-benzenesulfonamide

: 487-79-6
(-)-kainic acid

Guidance literature:: Multi-step reaction with 11 steps

1: 2) trimethylamine N-oxide / 1) CH₂Cl₂

2: H₂ / Pd/C / ethyl acetate / 760 Torr

3: 95 percent / FeCl₃, EtMgBr / diethyl ether; tetrahydrofuran / Ambient temperature

4: 1) O₃, 2) Me₂S

5: 90 percent

6: 72 percent / tetrahydrofuran / 0 °C

7: CF₃COOH / CH₂Cl₂ / Ambient temperature

8: PDC / dimethylformamide / Ambient temperature

10: LiOH / methanol; H₂O / Ambient temperature

11: Li, NH₃ / tetrahydrofuran / -78 °C

With lithium hydroxide; dipyridinium dichromate; dimethylsulfide; trimethylamine-N-oxide; ethylmagnesium bromide; ammonia; hydrogen; iron(III) chloride; lithium; ozone; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)79176-3