trityl-(3-{6-[3-(trityl-amino)-propyl]-[1,6]diazecan-1-yl}-propyl)-amine

Base Information

Chemical Name:trityl-(3-{6-[3-(trityl-amino)-propyl]-[1,6]diazecan-1-yl}-propyl)-amine
CAS No.:450408-98-7
Molecular Formula:C₅₂H₆₀N₄
Molecular Weight:741.075
Hs Code.:

Synonyms:trityl-(3-{6-[3-(trityl-amino)-propyl]-[1,6]diazecan-1-yl}-propyl)-amine

Suppliers and Price of trityl-(3-{6-[3-(trityl-amino)-propyl]-[1,6]diazecan-1-yl}-propyl)-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of trityl-(3-{6-[3-(trityl-amino)-propyl]-[1,6]diazecan-1-yl}-propyl)-amine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of trityl-(3-{6-[3-(trityl-amino)-propyl]-[1,6]diazecan-1-yl}-propyl)-amine

There total 3 articles about trityl-(3-{6-[3-(trityl-amino)-propyl]-[1,6]diazecan-1-yl}-propyl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 450408-96-5
1,6-bis-[3-(trityl-amino)-propyl]-[1,6]diazecane-2,5-dione

: 450408-98-7
trityl-(3-{6-[3-(trityl-amino)-propyl]-[1,6]diazecan-1-yl}-propyl)-amine

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 5h; Heating;
DOI:10.1016/S0040-4039(02)00335-0

Reference yield:

: 168699-01-2
N¹,N¹⁴-bis(triphenylmethyl)spermine

: 450408-98-7
trityl-(3-{6-[3-(trityl-amino)-propyl]-[1,6]diazecan-1-yl}-propyl)-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 55 percent / CH₂Cl₂ / 26 h / 0 - 25 °C

2: 57 percent / bromotripyrrolidinophosphonium hexafluorophosphate; iPr₂NEt / CHCl₃ / 48 h / 25 °C

3: 78 percent / LiAlH₄ / tetrahydrofuran / 5 h / Heating

With lithium aluminium tetrahydride; N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In tetrahydrofuran; dichloromethane; chloroform;
DOI:10.1016/S0040-4039(02)00335-0

Reference yield:

: 450408-95-4
N-[3-(trityl-amino)-propyl]-N-{4-[3-(trityl-amino)-propylamino]-butyl}-succinamic acid

: 450408-98-7
trityl-(3-{6-[3-(trityl-amino)-propyl]-[1,6]diazecan-1-yl}-propyl)-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / bromotripyrrolidinophosphonium hexafluorophosphate; iPr₂NEt / CHCl₃ / 48 h / 25 °C

2: 78 percent / LiAlH₄ / tetrahydrofuran / 5 h / Heating

With lithium aluminium tetrahydride; N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In tetrahydrofuran; chloroform;
DOI:10.1016/S0040-4039(02)00335-0