Technology Process of C19H18BrN3O4S
There total 12 articles about C19H18BrN3O4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium sulfite / water; ethanol / 15 h / 70 °C / Inert atmosphere; Sealed tube
2: thionyl chloride; N,N-dimethyl-formamide / toluene / 4 h / Inert atmosphere; Sealed tube; Reflux
3: ammonium hydroxide / tetrahydrofuran; toluene; water / 2 h / -10 °C / Inert atmosphere; Sealed tube
4: hydrogen iodide / water / 4 h / 90 °C / Inert atmosphere; Sealed tube
5: triethylamine / acetone / 0.5 h / 0 °C / Inert atmosphere; Sealed tube
6: potassium carbonate / water / 2 h / Inert atmosphere; Sealed tube; Reflux
With
ammonium hydroxide; thionyl chloride; hydrogen iodide; potassium carbonate; triethylamine; N,N-dimethyl-formamide; sodium sulfite;
In
tetrahydrofuran; ethanol; water; acetone; toluene;
- Guidance literature:
-
With
potassium carbonate;
In
water;
for 2h;
Inert atmosphere;
Sealed tube;
Reflux;
- Guidance literature:
-
With
potassium carbonate;
In
water;
for 2h;
Reflux;