2,4,6-tris[(E)-2-{4-[(diethoxyphosphoryl)methyl]phenyl}ethenyl]-1,3,5-triazine

Base Information

Chemical Name:2,4,6-tris[(E)-2-{4-[(diethoxyphosphoryl)methyl]phenyl}ethenyl]-1,3,5-triazine
CAS No.:642471-70-3
Molecular Formula:C₄₂H₅₄N₃O₉P₃
Molecular Weight:837.827
Hs Code.:

Synonyms:2,4,6-tris[(E)-2-{4-[(diethoxyphosphoryl)methyl]phenyl}ethenyl]-1,3,5-triazine

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Chemical Property of 2,4,6-tris[(E)-2-{4-[(diethoxyphosphoryl)methyl]phenyl}ethenyl]-1,3,5-triazine

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Technology Process of 2,4,6-tris[(E)-2-{4-[(diethoxyphosphoryl)methyl]phenyl}ethenyl]-1,3,5-triazine

There total 5 articles about 2,4,6-tris[(E)-2-{4-[(diethoxyphosphoryl)methyl]phenyl}ethenyl]-1,3,5-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.9%

: 78-40-0
triethyl phosphate

: 2,4,6-Tris-[(E)-2-(4-bromomethyl-phenyl)-vinyl]-[1,3,5]triazine

: 642471-70-3
2,4,6-tris[(E)-2-{4-[(diethoxyphosphoryl)methyl]phenyl}ethenyl]-1,3,5-triazine

Guidance literature:: at 150 ℃; for 5h;
DOI:10.1002/cjoc.201180369

Reference yield:

: 823-94-9
2,4,6-trimethyl-s-triazine

: 642471-70-3
2,4,6-tris[(E)-2-{4-[(diethoxyphosphoryl)methyl]phenyl}ethenyl]-1,3,5-triazine

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / KOH / methanol / Heating

2: NBS; AIBN / CCl₄ / Heating

3: 300 mg / 5 h / 150 °C

With potassium hydroxide; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In methanol; tetrachloromethane; 2: Wohl-Ziegler reaction / 3: Wittig-Horner reaction;
DOI:10.1002/ejoc.200300132

Reference yield:

: 104-87-0
4-methyl-benzaldehyde

: 642471-70-3
2,4,6-tris[(E)-2-{4-[(diethoxyphosphoryl)methyl]phenyl}ethenyl]-1,3,5-triazine

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / KOH / methanol / Heating

2: NBS; AIBN / CCl₄ / Heating

3: 300 mg / 5 h / 150 °C

With potassium hydroxide; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In methanol; tetrachloromethane; 2: Wohl-Ziegler reaction / 3: Wittig-Horner reaction;
DOI:10.1002/ejoc.200300132