N--4-chlorobenzenesulfonamide

Base Information

Chemical Name:N--4-chlorobenzenesulfonamide
CAS No.:13068-12-7
Molecular Formula:C₉H₁₀ClNO₂S₃
Molecular Weight:295.835
Hs Code.:

N-<bis(methylthio)methylene>-4-chlorobenzenesulfonamide

Synonyms:N--4-chlorobenzenesulfonamide

Suppliers and Price of N--4-chlorobenzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of N--4-chlorobenzenesulfonamide

Chemical Property:

Purity/Quality:

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Technology Process of N--4-chlorobenzenesulfonamide

There total 6 articles about N--4-chlorobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 75-15-0,12122-00-8
carbon disulfide

: 98-64-6
4-Chlorobenzenesulfonamide

: 74-88-4
methyl iodide

: 13068-12-7
N--4-chlorobenzenesulfonamide

Guidance literature:: carbon disulfide; 4-Chlorobenzenesulfonamide; With potassium hydroxide; In water; N,N-dimethyl-formamide; Inert atmosphere; Cooling with ice;

methyl iodide; In water; N,N-dimethyl-formamide; at 10 - 20 ℃; Inert atmosphere;
DOI:10.1021/jm200466r

Reference yield:

: 75-15-0,12122-00-8
carbon disulfide

: 98-64-6
4-Chlorobenzenesulfonamide

: 77-78-1
dimethyl sulfate

: 13068-12-7
N--4-chlorobenzenesulfonamide

Guidance literature:: With sodium hydroxide; Yield given. Multistep reaction; 1.) DMF, r.t., 2 h, 2.) r.t., 2 h;
DOI:10.1055/s-1991-26426

Reference yield:

: 98-64-6
4-Chlorobenzenesulfonamide

: 13068-12-7
N--4-chlorobenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOH / dimethylformamide / 0.58 h / Ambient temperature

2: aq. NaOH / dimethylformamide / 1 h

With sodium hydroxide; In N,N-dimethyl-formamide;