Technology Process of C26H30BNO6
There total 9 articles about C26H30BNO6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C32H44BNO6Si;
With
toluene-4-sulfonic acid;
In
tetrahydrofuran; water;
at 23 ℃;
for 14h;
Inert atmosphere;
With
2,3-dimethyl-2,3-butane diol; triethylamine;
In
tetrahydrofuran; water;
at 23 ℃;
for 24h;
Inert atmosphere;
DOI:10.1021/jo400105m
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: diphenylphosphoranyl azide; triethylamine / benzene / 1 h / 85 °C / Inert atmosphere
1.2: 3 h / 85 °C / Inert atmosphere
2.1: toluene-4-sulfonic acid / tetrahydrofuran; water / 14 h / 23 °C / Inert atmosphere
2.2: 24 h / 23 °C / Inert atmosphere
With
diphenylphosphoranyl azide; toluene-4-sulfonic acid; triethylamine;
In
tetrahydrofuran; water; benzene;
1.1: |Curtius Rearrangement / 1.2: |Curtius Rearrangement;
DOI:10.1021/jo400105m
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; 1,1'-bis-(diphenylphosphino)ferrocene; potassium acetate / 1,4-dioxane / 48 h / 80 °C / Inert atmosphere
2.1: diphenylphosphoranyl azide; triethylamine / benzene / 1 h / 85 °C / Inert atmosphere
2.2: 3 h / 85 °C / Inert atmosphere
3.1: toluene-4-sulfonic acid / tetrahydrofuran; water / 14 h / 23 °C / Inert atmosphere
3.2: 24 h / 23 °C / Inert atmosphere
With
1,1'-bis-(diphenylphosphino)ferrocene; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; diphenylphosphoranyl azide; potassium acetate; toluene-4-sulfonic acid; triethylamine;
In
tetrahydrofuran; 1,4-dioxane; water; benzene;
1.1: |Miyaura Borylation Reaction / 2.1: |Curtius Rearrangement / 2.2: |Curtius Rearrangement;
DOI:10.1021/jo400105m
