Technology Process of C35H34N4NiO2
There total 3 articles about C35H34N4NiO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tert.-butyl lithium / diethyl ether; pentane / 2 h / -78 °C / Inert atmosphere
1.2: 3.08 h / -78 - 20 °C / Inert atmosphere
2.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / tetrahydrofuran; diethyl ether; pentane / 12 h / 0 - 20 °C / Inert atmosphere
3.1: nickel(II) acetate tetrahydrate / N,N-dimethyl-formamide / 2 h / 140 °C
With
water; tert.-butyl lithium; nickel(II) acetate tetrahydrate; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide; pentane;
DOI:10.1016/j.tetlet.2011.08.025
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tert.-butyl lithium / diethyl ether; pentane / 2 h / -78 °C / Inert atmosphere
1.2: 3.08 h / -78 - 20 °C / Inert atmosphere
2.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / tetrahydrofuran; diethyl ether; pentane / 12 h / 0 - 20 °C / Inert atmosphere
3.1: nickel(II) acetate tetrahydrate / N,N-dimethyl-formamide / 2 h / 140 °C
With
water; tert.-butyl lithium; nickel(II) acetate tetrahydrate; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide; pentane;
DOI:10.1016/j.tetlet.2011.08.025
