(S)-FMOC-3-AMINO-2-(PHENYLSULFONYLAMINO)-PROPIONIC ACID

Base Information

• Chemical Name: (S)-FMOC-3-AMINO-2-(PHENYLSULFONYLAMINO)-PROPIONIC ACID
• CAS No.: 273399-94-3
• Molecular Formula: C24H22 N2 O6 S
• Molecular Weight: 466.51
• Mol file: 273399-94-3.mol

Synonyms:FMOC-(S)-3-AMINO-2-(PHENYLSULFONYLAMINO)-PROPIONIC ACID;(S)-FMOC-3-AMINO-2-(PHENYLSULFONYLAMINO)-PROPIONIC ACID

Chemical Property of (S)-FMOC-3-AMINO-2-(PHENYLSULFONYLAMINO)-PROPIONIC ACID

Chemical Property:

• PKA: 3.12±0.10(Predicted)
• PSA: 130.18000
• Density: 1.381±0.06 g/cm3(Predicted)
• LogP: 4.81940
• Storage Temp.: Store at?0-5°C

Purity/Quality:

98% ^*data from raw suppliers

Fmoc-(s)-3-amino-2-(phenylsulfonylamino)-propionicacid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (S)-FMOC-3-AMINO-2-(PHENYLSULFONYLAMINO)-PROPIONIC ACID

There total 1 articles about (S)-FMOC-3-AMINO-2-(PHENYLSULFONYLAMINO)-PROPIONIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide (82911-69-1) + 3-amino-2(S)-phenylsulfonylaminopropionic acid (156185-88-5) → N3-Fmoc-N2-benzenesulfonyl-L-2,3-diaminopropionic acid (273399-94-3)

Guidance literature:

N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide; 3-amino-2(S)-phenylsulfonylaminopropionic acid; With sodium hydrogencarbonate; In water; acetone; at 0 ℃; for 23h;

With water; acetic acid; In ethyl acetate;

Reference yield:

2-chlorotrityl chloride polystyrene resin + N3-Fmoc-N2-benzenesulfonyl-L-2,3-diaminopropionic acid (273399-94-3) → C43H34ClN2O6PolS

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; for 0.5h; not specified

Reference yield:

N-{[(9H-fluoren-9-yl)methoxy]carbonyl}-3-methyl-L-phenylalanine (211637-74-0,352351-64-5) + N3-Fmoc-N2-benzenesulfonyl-L-2,3-diaminopropionic acid (273399-94-3) + C26H25NO4 → C30H36N4O6S

Guidance literature:

N-{[(9H-fluoren-9-yl)methoxy]carbonyl}-3-methyl-L-phenylalanine; With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 2h;

With piperidine; In N,N-dimethyl-formamide; for 0.5h;

N₃-Fmoc-N₂-benzenesulfonyl-L-2,3-diaminopropionic acid; C₂₆H₂₅NO₄; Further stages;

DOI:10.1002/anie.202005070

upstream raw materials:

N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

3-amino-2(S)-phenylsulfonylaminopropionic acid

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