3--2-oxo-1-tert-butyldimethylsilyloxy propane

Base Information

Chemical Name:3--2-oxo-1-tert-butyldimethylsilyloxy propane
CAS No.:160193-12-4
Molecular Formula:C₁₅H₂₄O₂Si
Molecular Weight:264.44
Hs Code.:

3-<phenyl>-2-oxo-1-tert-butyldimethylsilyloxy propane

Synonyms:3--2-oxo-1-tert-butyldimethylsilyloxy propane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3--2-oxo-1-tert-butyldimethylsilyloxy propane

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Technology Process of 3--2-oxo-1-tert-butyldimethylsilyloxy propane

There total 13 articles about 3--2-oxo-1-tert-butyldimethylsilyloxy propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 121618-58-4,121701-48-2,145032-20-8
trans-tert-butyldimethyl(((2S,3S)-3-phenyloxiran-2-yl)methoxy)silane

: 160193-12-4
3--2-oxo-1-tert-butyldimethylsilyloxy propane

Guidance literature:: With [iron(III)(5,10,15,20-tetraphenyl-21H,23H-porphine)] perchlorate; In 1,4-dioxane; at 80 ℃; for 0.5h;
DOI:10.1246/cl.1996.1031

Reference yield: 99.0%

: 121618-58-4,121701-48-2,145032-20-8
trans-tert-butyldimethyl(((2S,3S)-3-phenyloxiran-2-yl)methoxy)silane

: 160193-12-4
3--2-oxo-1-tert-butyldimethylsilyloxy propane

: 186199-35-9
3-[(tert-butyldimethylsilyl)oxy]-2-phenylpropanal

Guidance literature:: With [iron(III)(5,10,15,20-tetraphenyl-21H,23H-porphine)] perchlorate; In 1,4-dioxane; at 80 ℃; Product distribution; var.cat.: Mn(tpp)ClO₄, but no reaction with Mn(tpp)Cl,Fe(tpp)Cl, and BF₃*Et₂O; var. solv. CH₂Cl₂, var. time 1 and 48 h;
DOI:10.1246/cl.1996.1031

Reference yield: 93.0%

: 121701-48-2
(1R,2R)-trans-2-[(tert-butyldimethylsilyloxy)methyl]-3-phenyloxirane

: 160193-12-4
3--2-oxo-1-tert-butyldimethylsilyloxy propane

Guidance literature:: With gold(III) chloride; silver hexafluoroantimonate; In 1,4-dioxane; at 20 ℃; for 0.25h; regioselective reaction;
DOI:10.1016/j.tetlet.2012.07.056