1-benzo[1,3]dioxol-5-yl-cyclopropanecarboxylic acid 4'-[bis-(4-methoxyphenyl)-methylsulfanyl]-6-methylbiphenyl-3-ylamide

Base Information

Chemical Name:1-benzo[1,3]dioxol-5-yl-cyclopropanecarboxylic acid 4'-[bis-(4-methoxyphenyl)-methylsulfanyl]-6-methylbiphenyl-3-ylamide
CAS No.:945244-21-3
Molecular Formula:C₃₉H₃₅NO₅S
Molecular Weight:629.777
Hs Code.:

Synonyms:1-benzo[1,3]dioxol-5-yl-cyclopropanecarboxylic acid 4'-[bis-(4-methoxyphenyl)-methylsulfanyl]-6-methylbiphenyl-3-ylamide

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Chemical Property of 1-benzo[1,3]dioxol-5-yl-cyclopropanecarboxylic acid 4'-[bis-(4-methoxyphenyl)-methylsulfanyl]-6-methylbiphenyl-3-ylamide

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Technology Process of 1-benzo[1,3]dioxol-5-yl-cyclopropanecarboxylic acid 4'-[bis-(4-methoxyphenyl)-methylsulfanyl]-6-methylbiphenyl-3-ylamide

There total 6 articles about 1-benzo[1,3]dioxol-5-yl-cyclopropanecarboxylic acid 4'-[bis-(4-methoxyphenyl)-methylsulfanyl]-6-methylbiphenyl-3-ylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 862574-89-8
1-(2H-1,3-benzodioxol-5-yl)cyclopropane-1-carboxylic acid

: 945244-20-2
4'-[bis-(4-methoxyphenyl)methylsulfanyl]-6-methylbiphenyl-3-ylamine

: 945244-21-3
1-benzo[1,3]dioxol-5-yl-cyclopropanecarboxylic acid 4'-[bis-(4-methoxyphenyl)-methylsulfanyl]-6-methylbiphenyl-3-ylamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In chloroform; at 65 ℃; for 48h;

Reference yield:

: 4439-02-5
3,4-methylenedioxyphenylacetonitrile

: 945244-21-3
1-benzo[1,3]dioxol-5-yl-cyclopropanecarboxylic acid 4'-[bis-(4-methoxyphenyl)-methylsulfanyl]-6-methylbiphenyl-3-ylamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; sodium hydroxide; sodium chloride; N-benzyl-N,N,N-triethylammonium chloride / dichloromethane

2: DIEA / chloroform

With hydrogenchloride; sodium hydroxide; DIEA; sodium chloride; N-benzyl-N,N,N-triethylammonium chloride; In dichloromethane; chloroform;

Reference yield:

: 728-87-0
4,4'-Dimethoxybenzhydrol

: 945244-21-3
1-benzo[1,3]dioxol-5-yl-cyclopropanecarboxylic acid 4'-[bis-(4-methoxyphenyl)-methylsulfanyl]-6-methylbiphenyl-3-ylamide

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / 1 h / 60 °C

2: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile / 0.11 h / 160 °C / Microwave irradiation

3: N-ethyl-N,N-diisopropylamine / chloroform / 48 h / 65 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; In chloroform; acetonitrile;