(R)-methyl 3-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyloxy)-2-methylpropanoate

Base Information

Chemical Name:(R)-methyl 3-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyloxy)-2-methylpropanoate
CAS No.:1190373-42-2
Molecular Formula:C₃₉H₄₄O₈
Molecular Weight:640.774
Hs Code.:

Synonyms:(R)-methyl 3-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyloxy)-2-methylpropanoate

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Chemical Property of (R)-methyl 3-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyloxy)-2-methylpropanoate

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Technology Process of (R)-methyl 3-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyloxy)-2-methylpropanoate

There total 1 articles about (R)-methyl 3-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyloxy)-2-methylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 72657-23-9,42998-03-8
methyl (R)-3-hydroxy-2-methylpropionate

: 74808-09-6,90357-89-4,90358-01-3,103368-01-0,103368-04-3,103368-06-5,104048-30-8,104048-33-1,114743-70-3,132201-75-3,132748-02-8,83441-60-5
2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl trichloroacetimidate

: 1190373-42-2
(R)-methyl 3-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyloxy)-2-methylpropanoate

: 1190373-30-8
(R)-methyl 3-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyloxy)-2-methylpropanoate

Guidance literature:: methyl (R)-3-hydroxy-2-methylpropionate; 2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl trichloroacetimidate; With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 2.25h; Inert atmosphere;

In diethyl ether; Petroleum ether; Resolution of racemate;
DOI:10.1016/j.bmc.2009.06.016

Reference yield: 83.0%

: 1190373-42-2
(R)-methyl 3-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyloxy)-2-methylpropanoate

: 1190373-45-5
(R)-3-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyloxy)-2-methylpropanoic acid

Guidance literature:: (R)-methyl 3-(2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyloxy)-2-methylpropanoate; With water; sodium hydroxide; In 1,4-dioxane; at 20 ℃; for 24h;

With hydrogenchloride; water; In 1,4-dioxane;
DOI:10.1016/j.bmc.2009.06.016