N-benzyloxycarbonyl-3-(6-bromo-4-oxoquinazolin-3(4H)-yl)-4-methylaniline

Base Information

Chemical Name:N-benzyloxycarbonyl-3-(6-bromo-4-oxoquinazolin-3(4H)-yl)-4-methylaniline
CAS No.:872091-91-3
Molecular Formula:C₂₃H₁₈BrN₃O₃
Molecular Weight:464.318
Hs Code.:

Synonyms:N-benzyloxycarbonyl-3-(6-bromo-4-oxoquinazolin-3(4H)-yl)-4-methylaniline

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Chemical Property of N-benzyloxycarbonyl-3-(6-bromo-4-oxoquinazolin-3(4H)-yl)-4-methylaniline

Chemical Property:

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Technology Process of N-benzyloxycarbonyl-3-(6-bromo-4-oxoquinazolin-3(4H)-yl)-4-methylaniline

There total 4 articles about N-benzyloxycarbonyl-3-(6-bromo-4-oxoquinazolin-3(4H)-yl)-4-methylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 872091-90-2
3-(6-bromo-4-oxoquinazolin-3(4H)-yl)-4-methylbenzoic acid

: 100-51-6,185532-71-2
benzyl alcohol

: 872091-91-3
N-benzyloxycarbonyl-3-(6-bromo-4-oxoquinazolin-3(4H)-yl)-4-methylaniline

Guidance literature:: With diphenyl phosphoryl azide; triethylamine; In toluene; for 12h; Heating / reflux;

Reference yield:

: 18595-18-1
3-amino-4-methyl benzoic acid methyl ester

: 872091-91-3
N-benzyloxycarbonyl-3-(6-bromo-4-oxoquinazolin-3(4H)-yl)-4-methylaniline

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / toluene / 3 h / Heating / reflux

1.2: 20 h / 40 °C / Heating / reflux

2.1: hydrogenchloride; water / 6 h / Heating / reflux

3.1: diphenyl phosphoryl azide; triethylamine / toluene / 12 h / Heating / reflux

With hydrogenchloride; diphenyl phosphoryl azide; water; triethylamine; acetic acid; In toluene;

Reference yield:

: 5794-88-7
5-Bromo-2-aminobenzoic acid

: 872091-91-3
N-benzyloxycarbonyl-3-(6-bromo-4-oxoquinazolin-3(4H)-yl)-4-methylaniline

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / toluene / 3 h / Heating / reflux

1.2: 20 h / 40 °C / Heating / reflux

2.1: hydrogenchloride; water / 6 h / Heating / reflux

3.1: diphenyl phosphoryl azide; triethylamine / toluene / 12 h / Heating / reflux

With hydrogenchloride; diphenyl phosphoryl azide; water; triethylamine; acetic acid; In toluene;