4-Acetylamino-benzenesulfonic acid (E)-5,9-dimethyl-deca-5,9-dienyl ester

Base Information

Chemical Name:4-Acetylamino-benzenesulfonic acid (E)-5,9-dimethyl-deca-5,9-dienyl ester
CAS No.:192133-75-8
Molecular Formula:C₂₀H₂₉NO₄S
Molecular Weight:379.521
Hs Code.:

Synonyms:4-Acetylamino-benzenesulfonic acid (E)-5,9-dimethyl-deca-5,9-dienyl ester

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Chemical Property of 4-Acetylamino-benzenesulfonic acid (E)-5,9-dimethyl-deca-5,9-dienyl ester

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Technology Process of 4-Acetylamino-benzenesulfonic acid (E)-5,9-dimethyl-deca-5,9-dienyl ester

There total 5 articles about 4-Acetylamino-benzenesulfonic acid (E)-5,9-dimethyl-deca-5,9-dienyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99701-65-2
6-(benzyloxy)hexan-2-one

: 192133-75-8
4-Acetylamino-benzenesulfonic acid (E)-5,9-dimethyl-deca-5,9-dienyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 74 percent / tetrahydrofuran; diethyl ether / 0 deg C, 2 h, rt, 3.5 h

2: PBr₃ / pyridine; hexane / -10 deg C to rt, 1.5 h

3: Mg / tetrahydrofuran / 0.5 h, reflux; overnight, rt

4: 100 percent / Na, NH₃ / diethyl ether / 0.5 h / -78 °C

5: DMAP / pyridine / 5 h

With dmap; ammonia; sodium; phosphorus tribromide; magnesium; In tetrahydrofuran; pyridine; diethyl ether; hexane;
DOI:10.1021/ja970675a

Reference yield:

: 192133-78-1
7-Benzyloxy-3-methyl-hept-1-en-3-ol

: 192133-75-8
4-Acetylamino-benzenesulfonic acid (E)-5,9-dimethyl-deca-5,9-dienyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: PBr₃ / pyridine; hexane / -10 deg C to rt, 1.5 h

2: Mg / tetrahydrofuran / 0.5 h, reflux; overnight, rt

3: 100 percent / Na, NH₃ / diethyl ether / 0.5 h / -78 °C

4: DMAP / pyridine / 5 h

With dmap; ammonia; sodium; phosphorus tribromide; magnesium; In tetrahydrofuran; pyridine; diethyl ether; hexane;
DOI:10.1021/ja970675a

Reference yield:

: 192133-79-2
((Z)-7-Bromo-5-methyl-hept-5-enyloxymethyl)-benzene

: 192133-75-8
4-Acetylamino-benzenesulfonic acid (E)-5,9-dimethyl-deca-5,9-dienyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Mg / tetrahydrofuran / 0.5 h, reflux; overnight, rt

2: 100 percent / Na, NH₃ / diethyl ether / 0.5 h / -78 °C

3: DMAP / pyridine / 5 h

With dmap; ammonia; sodium; magnesium; In tetrahydrofuran; pyridine; diethyl ether;
DOI:10.1021/ja970675a