methyl 6-(N-benzenesulfonylamino)-N,O-isopropylidene-2,3,6,8-tetradeoxy-α-D-erythrooct-2-enopyranos-4-uloside

Base Information

Chemical Name:methyl 6-(N-benzenesulfonylamino)-N,O-isopropylidene-2,3,6,8-tetradeoxy-α-D-erythrooct-2-enopyranos-4-uloside
CAS No.:142037-59-0
Molecular Formula:C₁₈H₂₃NO₆S
Molecular Weight:381.45
Hs Code.:

Synonyms:methyl 6-(N-benzenesulfonylamino)-N,O-isopropylidene-2,3,6,8-tetradeoxy-α-D-erythrooct-2-enopyranos-4-uloside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 6-(N-benzenesulfonylamino)-N,O-isopropylidene-2,3,6,8-tetradeoxy-α-D-erythrooct-2-enopyranos-4-uloside

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Technology Process of methyl 6-(N-benzenesulfonylamino)-N,O-isopropylidene-2,3,6,8-tetradeoxy-α-D-erythrooct-2-enopyranos-4-uloside

There total 2 articles about methyl 6-(N-benzenesulfonylamino)-N,O-isopropylidene-2,3,6,8-tetradeoxy-α-D-erythrooct-2-enopyranos-4-uloside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.5%

: 142037-63-6
6-amino-N-benzenesulfonyl-N,O-isopropylidene-2,3,6,8-tetradeoxy-α-D-ribo-oct-2-enopyranos-4-ulose

: 74-88-4
methyl iodide

: 142037-59-0
methyl 6-(N-benzenesulfonylamino)-N,O-isopropylidene-2,3,6,8-tetradeoxy-α-D-erythrooct-2-enopyranos-4-uloside

: methyl 6-amino-N-benzenesulfonyl-N,O-isopropylidene-2,3,6,8-tetradeoxy-β-D-ribo-oct-2-enopyranosid-4-ulose

Guidance literature:: With silver(l) oxide; In diethyl ether; at 25 ℃; for 24h;

Reference yield:

: 141990-12-7
(1R,2R,3R)-N-benzenesulfonyl-N,O³-isopropylidene-1-(2-furyl)-2-aminobutane-1,3-diol

: 142037-59-0
methyl 6-(N-benzenesulfonylamino)-N,O-isopropylidene-2,3,6,8-tetradeoxy-α-D-erythrooct-2-enopyranos-4-uloside

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / sodium hydrogen carbonate, m-chloroperbenzoic acid / CH₂Cl₂

2: 80 percent / Ag₂O / diethyl ether / 24 h / 25 °C

With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; silver(l) oxide; In diethyl ether; dichloromethane;