(1-Butyl-pentylsulfanyl)-benzene

Base Information

Chemical Name:(1-Butyl-pentylsulfanyl)-benzene
CAS No.:203638-65-7
Molecular Formula:C₁₅H₂₄S
Molecular Weight:236.422
Hs Code.:

Synonyms:(1-Butyl-pentylsulfanyl)-benzene

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Chemical Property of (1-Butyl-pentylsulfanyl)-benzene

Chemical Property:

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Technology Process of (1-Butyl-pentylsulfanyl)-benzene

There total 1 articles about (1-Butyl-pentylsulfanyl)-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 56651-45-7
Di-n-butylketon-diphenyl-dithioacetal

: 203638-65-7
(1-Butyl-pentylsulfanyl)-benzene

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide; tert-butyl alcohol; In benzene; for 73h; Ambient temperature;
DOI:10.1248/cpb.46.187

Reference yield:

: 203638-65-7
(1-Butyl-pentylsulfanyl)-benzene

: 502-56-7
nonanone-5

Guidance literature:: Multi-step reaction with 5 steps

1: m-chloroperbenzoic acid / CH₂Cl₂

2: 50 percent / butyl-lithium / hexane; tetrahydrofuran / 1 h / 0 °C

3: 86 percent / di-isobutylaluminum hydride / toluene / 48 h / Heating

4: 85percent m-chloroperbenzoic acid / CH₂Cl₂ / 1.5 h / -23 °C

5: 2.) 1 M mercury(II) acetate / 1.) THF, reflux, 4 h, 2.) THF, water, 17 h, room temperature

With n-butyllithium; diisobutylaluminum hydride; mercury(II) diacetate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; hexane; dichloromethane; toluene;
DOI:10.1039/P19860000195

Reference yield:

: 203638-65-7
(1-Butyl-pentylsulfanyl)-benzene

: 3657-08-7
nonan-5-one-(2,4-dinitro-phenylhydrazone)

Guidance literature:: Multi-step reaction with 5 steps

1: m-chloroperbenzoic acid / CH₂Cl₂

2: 50 percent / butyl-lithium / hexane; tetrahydrofuran / 1 h / 0 °C

3: 86 percent / di-isobutylaluminum hydride / toluene / 48 h / Heating

4: 85percent m-chloroperbenzoic acid / CH₂Cl₂ / 1.5 h / -23 °C

With n-butyllithium; diisobutylaluminum hydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; hexane; dichloromethane; toluene;
DOI:10.1039/P19860000195