Technology Process of C32H32ClN5
There total 11 articles about C32H32ClN5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydroxide;
In
water; acetone;
at 55 - 60 ℃;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: ethyl acetate / 3 h / 25 - 30 °C
2: potassium carbonate / ethyl acetate; water / pH 9 - 10
3: potassium carbonate / acetonitrile; N,N-dimethyl-formamide / 6 h / 70 - 75 °C
4: sodium hydroxide / water; acetone / 55 - 60 °C
With
potassium carbonate; sodium hydroxide;
In
water; ethyl acetate; N,N-dimethyl-formamide; acetone; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 60 - 70 °C / Inert atmosphere
2: ethyl acetate / 3 h / 25 - 30 °C
3: potassium carbonate / ethyl acetate; water / pH 9 - 10
4: potassium carbonate / acetonitrile; N,N-dimethyl-formamide / 6 h / 70 - 75 °C
5: sodium hydroxide / water; acetone / 55 - 60 °C
With
lithium aluminium tetrahydride; potassium carbonate; sodium hydroxide;
In
tetrahydrofuran; water; ethyl acetate; N,N-dimethyl-formamide; acetone; acetonitrile;