methyl 2'-hydroxyphenyl-12-bromo-13,14-imidazolyl-deisopropyldehydroabietate

Base Information

Chemical Name:methyl 2'-hydroxyphenyl-12-bromo-13,14-imidazolyl-deisopropyldehydroabietate
CAS No.:1123216-99-8
Molecular Formula:C₂₅H₂₇BrN₂O₃
Molecular Weight:483.405
Hs Code.:

Synonyms:methyl 2'-hydroxyphenyl-12-bromo-13,14-imidazolyl-deisopropyldehydroabietate

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Chemical Property of methyl 2'-hydroxyphenyl-12-bromo-13,14-imidazolyl-deisopropyldehydroabietate

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Technology Process of methyl 2'-hydroxyphenyl-12-bromo-13,14-imidazolyl-deisopropyldehydroabietate

There total 4 articles about methyl 2'-hydroxyphenyl-12-bromo-13,14-imidazolyl-deisopropyldehydroabietate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.4%

: 90-02-8
salicylaldehyde

: 671820-50-1
methyl 12-bromo-13,14-diaminodeisopropyldehydroabietate

: 1123216-99-8
methyl 2'-hydroxyphenyl-12-bromo-13,14-imidazolyl-deisopropyldehydroabietate

Guidance literature:: With air; In 1,4-dioxane; for 5h; Reflux;
DOI:10.3390/molecules16010100

Reference yield:

: 1740-19-8
dehydroabietic acid

: 1123216-99-8
methyl 2'-hydroxyphenyl-12-bromo-13,14-imidazolyl-deisopropyldehydroabietate

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate; p-toluenesulfonyl chloride

2: N-Bromosuccinimide

3: sulfuric acid; nitric acid

4: 10% palladium on activated charcoal; hydrogen / ethanol

5: air / 1,4-dioxane / 5 h / Reflux

With N-Bromosuccinimide; sulfuric acid; 10% palladium on activated charcoal; hydrogen; nitric acid; potassium carbonate; p-toluenesulfonyl chloride; In 1,4-dioxane; ethanol;
DOI:10.3390/molecules16010100

Reference yield:

: 1235-74-1,1757-97-7,2756-34-5,7151-00-0,10178-27-5,10178-29-7,21699-55-8,24035-60-7
Methyl dehydroabietate

: 1123216-99-8
methyl 2'-hydroxyphenyl-12-bromo-13,14-imidazolyl-deisopropyldehydroabietate

Guidance literature:: Multi-step reaction with 4 steps

1: N-Bromosuccinimide

2: sulfuric acid; nitric acid

3: 10% palladium on activated charcoal; hydrogen / ethanol

4: air / 1,4-dioxane / 5 h / Reflux

With N-Bromosuccinimide; sulfuric acid; 10% palladium on activated charcoal; hydrogen; nitric acid; In 1,4-dioxane; ethanol;
DOI:10.3390/molecules16010100