6-(4-(4-methyl-1H-5-carbonylazide-1,2,3-triazol-1-yl)phenylamino)phenyl-N⁽²⁾,N⁽⁴⁾-bis(4-methoxyphenyl)-1,3,5-triazin-2,4-diamine

Base Information

• Chemical Name: 6-(4-(4-methyl-1H-5-carbonylazide-1,2,3-triazol-1-yl)phenylamino)phenyl-N⁽²⁾,N⁽⁴⁾-bis(4-methoxyphenyl)-1,3,5-triazin-2,4-diamine
• CAS No.: 1418000-01-7
• Molecular Formula: C₂₇H₂₄N₁₂O₃
• Molecular Weight: 564.566

Synonyms:6-(4-(4-methyl-1H-5-carbonylazide-1,2,3-triazol-1-yl)phenylamino)phenyl-N⁽²⁾,N⁽⁴⁾-bis(4-methoxyphenyl)-1,3,5-triazin-2,4-diamine

Chemical Property of 6-(4-(4-methyl-1H-5-carbonylazide-1,2,3-triazol-1-yl)phenylamino)phenyl-N⁽²⁾,N⁽⁴⁾-bis(4-methoxyphenyl)-1,3,5-triazin-2,4-diamine

Chemical Property:

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Safty Information:

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Technology Process of 6-(4-(4-methyl-1H-5-carbonylazide-1,2,3-triazol-1-yl)phenylamino)phenyl-N⁽²⁾,N⁽⁴⁾-bis(4-methoxyphenyl)-1,3,5-triazin-2,4-diamine

There total 5 articles about 6-(4-(4-methyl-1H-5-carbonylazide-1,2,3-triazol-1-yl)phenylamino)phenyl-N⁽²⁾,N⁽⁴⁾-bis(4-methoxyphenyl)-1,3,5-triazin-2,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

6-(4-(4-methyl-1H-5-carbonylchloride-1,2,3-triazol-1ylphenylamino)phenyl)-N(2),N(4)-bis(4-methoxyphenyl)-1,3,5-triazin-2,4-diamine (1418000-00-6) → 6-(4-(4-methyl-1H-5-carbonylazide-1,2,3-triazol-1-yl)phenylamino)phenyl-N(2),N(4)-bis(4-methoxyphenyl)-1,3,5-triazin-2,4-diamine (1418000-01-7)

Guidance literature:

With sodium azide; In pentane; at 20 ℃;

Reference yield:

4-methoxy-aniline (104-94-9) → 6-(4-(4-methyl-1H-5-carbonylazide-1,2,3-triazol-1-yl)phenylamino)phenyl-N(2),N(4)-bis(4-methoxyphenyl)-1,3,5-triazin-2,4-diamine (1418000-01-7)

Guidance literature:

Multi-step reaction with 6 steps

1.1: 3 h / 20 °C

2.1: sodium carbonate / 4 h / 35 - 50 °C

3.1: hydrogenchloride; sodium nitrite / water / 0.17 h / 0 °C

3.2: 3 h / 0 °C

4.1: sodium acetate / ethanol / 1 h / 20 °C

5.1: thionyl chloride / 2 h / Heating

6.1: sodium azide / pentane / 20 °C

With hydrogenchloride; thionyl chloride; sodium azide; sodium acetate; sodium carbonate; sodium nitrite; In ethanol; water; pentane;

Reference yield:

C23H21N9O2 (1417999-98-4) → 6-(4-(4-methyl-1H-5-carbonylazide-1,2,3-triazol-1-yl)phenylamino)phenyl-N(2),N(4)-bis(4-methoxyphenyl)-1,3,5-triazin-2,4-diamine (1418000-01-7)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium acetate / ethanol / 1 h / 20 °C

2: thionyl chloride / 2 h / Heating

3: sodium azide / pentane / 20 °C

With thionyl chloride; sodium azide; sodium acetate; In ethanol; pentane;

upstream raw materials:

C₂₃H₂₁N₉O₂

6-(4-(4-methyl-1H-5-carbonylchloride-1,2,3-triazol-1ylphenylamino)phenyl)-N⁽²⁾,N⁽⁴⁾-bis(4-methoxyphenyl)-1,3,5-triazin-2,4-diamine

4,6-dichloro-N-(4-methoxyphenyl)-1,3,5-triazin-2-amine

4-methoxy-aniline

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