[3-chloro-4-(pyrrolidin-1-ylmethyl)phenyl](3-chlorophenyl)methanone oxime

Base Information

Chemical Name:[3-chloro-4-(pyrrolidin-1-ylmethyl)phenyl](3-chlorophenyl)methanone oxime
CAS No.:1050527-69-9
Molecular Formula:C₁₈H₁₈Cl₂N₂O
Molecular Weight:349.26
Hs Code.:

Synonyms:[3-chloro-4-(pyrrolidin-1-ylmethyl)phenyl](3-chlorophenyl)methanone oxime

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Chemical Property of [3-chloro-4-(pyrrolidin-1-ylmethyl)phenyl](3-chlorophenyl)methanone oxime

Chemical Property:

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Technology Process of [3-chloro-4-(pyrrolidin-1-ylmethyl)phenyl](3-chlorophenyl)methanone oxime

There total 5 articles about [3-chloro-4-(pyrrolidin-1-ylmethyl)phenyl](3-chlorophenyl)methanone oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1050527-61-1
(3-chlorophenyl)(3-chloro-4-(pyrrolidin-1-ylmethyl)phenyl)methanone

: 1050527-69-9
[3-chloro-4-(pyrrolidin-1-ylmethyl)phenyl](3-chlorophenyl)methanone oxime

Guidance literature:: With hydroxylamine hydrochloride; barium carbonate; In methanol; for 18h; Reflux;

Reference yield:

: 89794-02-5
4-bromo-2-chlorotoluene

: 1050527-69-9
[3-chloro-4-(pyrrolidin-1-ylmethyl)phenyl](3-chlorophenyl)methanone oxime

Guidance literature:: Multi-step reaction with 4 steps

1.1: iodine; magnesium / tetrahydrofuran / Reflux

1.2: 4 h / 83 °C

2.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 4 h / Reflux

3.1: triethylamine / acetonitrile / 1 h / 0 °C

4.1: hydroxylamine hydrochloride; barium carbonate / methanol / 18 h / Reflux

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); hydroxylamine hydrochloride; iodine; magnesium; triethylamine; barium carbonate; In tetrahydrofuran; methanol; tetrachloromethane; acetonitrile;
DOI:10.1021/jm300802s

Reference yield:

: 1050527-48-4
(3-chlorophenyl)(4-methyl-3-chlorophenyl)methanone

: 1050527-69-9
[3-chloro-4-(pyrrolidin-1-ylmethyl)phenyl](3-chlorophenyl)methanone oxime

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / acetonitrile / 1 h / 0 °C

2: hydroxylamine hydrochloride; barium carbonate / methanol / 18 h / Reflux

With hydroxylamine hydrochloride; triethylamine; barium carbonate; In methanol; acetonitrile;
DOI:10.1021/jm300802s