(4S,5S)-5-[(E)-1-nonenyl]-2-pentyl-4-[(trityloxy)methyl]-4,5-dihydro-1,3-oxazole

Base Information

Chemical Name:(4S,5S)-5-[(E)-1-nonenyl]-2-pentyl-4-[(trityloxy)methyl]-4,5-dihydro-1,3-oxazole
CAS No.:254878-56-3
Molecular Formula:C₃₇H₄₇NO₂
Molecular Weight:537.786
Hs Code.:

Synonyms:(4S,5S)-5-[(E)-1-nonenyl]-2-pentyl-4-[(trityloxy)methyl]-4,5-dihydro-1,3-oxazole

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Chemical Property of (4S,5S)-5-[(E)-1-nonenyl]-2-pentyl-4-[(trityloxy)methyl]-4,5-dihydro-1,3-oxazole

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Technology Process of (4S,5S)-5-[(E)-1-nonenyl]-2-pentyl-4-[(trityloxy)methyl]-4,5-dihydro-1,3-oxazole

There total 5 articles about (4S,5S)-5-[(E)-1-nonenyl]-2-pentyl-4-[(trityloxy)methyl]-4,5-dihydro-1,3-oxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 254878-53-0
N-{(1S,2R,3E)-2-hydroxy-1-[(trityloxy)methyl]-3-undecenyl}hexanamide

: 254878-56-3
(4S,5S)-5-[(E)-1-nonenyl]-2-pentyl-4-[(trityloxy)methyl]-4,5-dihydro-1,3-oxazole

: 254878-55-2
N-{[1R,2E,4(RS)]-4-fluoro-1-[(trityloxy)methyl]-3-undecenyl}hexanamide

: N-{(1S,2R,3E)-2-fluoro-1-[(trityloxy)methyl]-3-undecenyl}hexanamide

: Hexanoic acid ((E)-(1S,2S)-2-fluoro-1-trityloxymethyl-undec-3-enyl)-amide

Guidance literature:: With 4,4'-diaminostilbene-2,2'-disulfonic acid; In dichloromethane; at -78 ℃; for 0.75h;
DOI:10.1021/jm000939v

Reference yield: 28.0%

: 254878-53-0
N-{(1S,2R,3E)-2-hydroxy-1-[(trityloxy)methyl]-3-undecenyl}hexanamide

: 254878-56-3
(4S,5S)-5-[(E)-1-nonenyl]-2-pentyl-4-[(trityloxy)methyl]-4,5-dihydro-1,3-oxazole

: 254878-55-2
N-{[1R,2E,4(RS)]-4-fluoro-1-[(trityloxy)methyl]-3-undecenyl}hexanamide

: 254878-54-1
N-{[1S,2(RS),3E]-2-fluoro-1-[(trityloxy)methyl]-3-undecenyl}hexanamide

Guidance literature:: With diethylamino-sulfur trifluoride; In dichloromethane; at -78 ℃;
DOI:10.1016/S0960-894X(99)00553-3

Reference yield:

: 241478-51-3
Hexanoic acid ((E)-(1S,2R)-2-hydroxy-1-hydroxymethyl-undec-3-enyl)-amide

: 254878-56-3
(4S,5S)-5-[(E)-1-nonenyl]-2-pentyl-4-[(trityloxy)methyl]-4,5-dihydro-1,3-oxazole

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / pyridine / 3 h / 100 °C

2: 14 percent / DAST / CH₂Cl₂ / 0.75 h / -78 °C

With pyridine; 4,4'-diaminostilbene-2,2'-disulfonic acid; In dichloromethane;
DOI:10.1021/jm000939v