N-[9-((4aR,7S,8aS)-2-Phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-9H-purin-6-yl]-benzamide

Base Information

Chemical Name:N-[9-((4aR,7S,8aS)-2-Phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-9H-purin-6-yl]-benzamide
CAS No.:176786-70-2
Molecular Formula:C₂₅H₂₃N₅O₄
Molecular Weight:457.489
Hs Code.:

Synonyms:N-[9-((4aR,7S,8aS)-2-Phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-9H-purin-6-yl]-benzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[9-((4aR,7S,8aS)-2-Phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-9H-purin-6-yl]-benzamide

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Technology Process of N-[9-((4aR,7S,8aS)-2-Phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-9H-purin-6-yl]-benzamide

There total 1 articles about N-[9-((4aR,7S,8aS)-2-Phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-9H-purin-6-yl]-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 98-88-4
benzoyl chloride

: 152613-21-3
1,5-anhydro-4,6-O-benzylidene-2-(adenin-9-yl)-2,3-dideoxy-D-arabino-hexitol

: 176786-70-2
N-[9-((4aR,7S,8aS)-2-Phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-9H-purin-6-yl]-benzamide

Guidance literature:: With pyridine; for 4h; Ambient temperature;
DOI:10.1002/chem.19970030118

Reference yield: 71.0%

: 176786-70-2
N-[9-((4aR,7S,8aS)-2-Phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-9H-purin-6-yl]-benzamide

: 176786-71-3
N-[9-((3S,5S,6R)-5-Hydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl)-9H-purin-6-yl]-benzamide

Guidance literature:: With acetic acid; at 60 ℃; for 5h;
DOI:10.1002/chem.19970030118

Reference yield:

: 176786-70-2
N-[9-((4aR,7S,8aS)-2-Phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-9H-purin-6-yl]-benzamide

: Diisopropyl-phosphoramidous acid (2R,3S,5S)-5-(6-benzoylamino-purin-9-yl)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-pyran-3-yl ester 2-cyano-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / 80percent acetic acid / 5 h / 60 °C

2: 63 percent / pyridine / 16 h / Ambient temperature

3: 65 percent / N,N-diisopropylethylamine / CH₂Cl₂ / 3 h / Ambient temperature

With pyridine; acetic acid; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1002/chem.19970030118