Amino-[(R)-5-(tert-butyl-diphenyl-silanyloxymethyl)-pyrrolidin-(2E)-ylidene]-acetic acid ethyl ester

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Chemical Name:Amino-[(R)-5-(tert-butyl-diphenyl-silanyloxymethyl)-pyrrolidin-(2E)-ylidene]-acetic acid ethyl ester
CAS No.:170421-36-0
Molecular Formula:C₂₅H₃₄N₂O₃Si
Molecular Weight:438.642
Hs Code.:

Synonyms:Amino-[(R)-5-(tert-butyl-diphenyl-silanyloxymethyl)-pyrrolidin-(2E)-ylidene]-acetic acid ethyl ester

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Chemical Property of Amino-[(R)-5-(tert-butyl-diphenyl-silanyloxymethyl)-pyrrolidin-(2E)-ylidene]-acetic acid ethyl ester

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Technology Process of Amino-[(R)-5-(tert-butyl-diphenyl-silanyloxymethyl)-pyrrolidin-(2E)-ylidene]-acetic acid ethyl ester

There total 4 articles about Amino-[(R)-5-(tert-butyl-diphenyl-silanyloxymethyl)-pyrrolidin-(2E)-ylidene]-acetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 157825-36-0
[(R)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-pyrrolidin-(2Z)-ylidene]-nitro-acetic acid ethyl ester

: 170421-36-0
Amino-[(R)-5-(tert-butyl-diphenyl-silanyloxymethyl)-pyrrolidin-(2E)-ylidene]-acetic acid ethyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In toluene; under 3800 Torr;
DOI:10.1016/S0040-4039(00)76798-0

Reference yield:

: ethyl (R)-2-[5-(tert-butyldiphenylsiloxymethyl)pyrrolidin-2-ylidene]-2-nitroacetate

: 170421-36-0
Amino-[(R)-5-(tert-butyl-diphenyl-silanyloxymethyl)-pyrrolidin-(2E)-ylidene]-acetic acid ethyl ester

Guidance literature:: With formic acid; triethylamine; palladium on activated charcoal; In methanol; at 20 ℃;
DOI:10.1016/S0040-4020(03)00377-6

Reference yield:

: 138629-44-4
(R)-5-(tert-butyl-diphenyl-silanyloxymethyl)-pyrrolidin-2-one

: 170421-36-0
Amino-[(R)-5-(tert-butyl-diphenyl-silanyloxymethyl)-pyrrolidin-(2E)-ylidene]-acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / benzene / 18 h / 60 °C

2: 65 percent / 8 h / 60 °C

3: HCO₂H; Et₃N / 10 percent Pd/C / methanol / 20 °C

With formic acid; triethylamine; palladium on activated charcoal; In methanol; benzene;
DOI:10.1016/S0040-4020(03)00377-6