Acetic acid, [(5R)-5-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-2-pyrrolidinylidene] nitro-, ethyl ester, (2Z)-

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Chemical Name:Acetic acid, [(5R)-5-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-2-pyrrolidinylidene] nitro-, ethyl ester, (2Z)-
CAS No.:157825-36-0
Molecular Formula:C25H32N2O5Si
Molecular Weight:468.625
Hs Code.:
Mol file:157825-36-0.mol

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Chemical Property of Acetic acid, [(5R)-5-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-2-pyrrolidinylidene] nitro-, ethyl ester, (2Z)-

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Technology Process of Acetic acid, [(5R)-5-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-2-pyrrolidinylidene] nitro-, ethyl ester, (2Z)-

There total 2 articles about Acetic acid, [(5R)-5-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-2-pyrrolidinylidene] nitro-, ethyl ester, (2Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 626-35-7
nitroacetic acid ethyl ester

: 157825-35-9
(R)-2-(tert-butyldiphenylsiloxymethyl)-5-methoxy-3,4-dihydro-2H-pyrrole

: 157825-36-0
[(R)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-pyrrolidin-(2Z)-ylidene]-nitro-acetic acid ethyl ester

Guidance literature:: at 60 ℃;
DOI:10.1016/S0040-4039(00)76798-0

Reference yield:

: 138629-44-4
(R)-5-(tert-butyl-diphenyl-silanyloxymethyl)-pyrrolidin-2-one

: 157825-36-0
[(R)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-pyrrolidin-(2Z)-ylidene]-nitro-acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / benzene / 60 °C

2: 67 percent / 60 °C

In benzene;
DOI:10.1016/S0040-4039(00)76798-0