5-(1,5-dimethyl-1-phenylselenohex-4-enyl)-2-methyl-2-vinyltetrahydrofuran

Base Information

Chemical Name:5-(1,5-dimethyl-1-phenylselenohex-4-enyl)-2-methyl-2-vinyltetrahydrofuran
CAS No.:82292-48-6
Molecular Formula:C₂₁H₃₀OSe
Molecular Weight:377.429
Hs Code.:

Synonyms:5-(1,5-dimethyl-1-phenylselenohex-4-enyl)-2-methyl-2-vinyltetrahydrofuran

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Chemical Property of 5-(1,5-dimethyl-1-phenylselenohex-4-enyl)-2-methyl-2-vinyltetrahydrofuran

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Technology Process of 5-(1,5-dimethyl-1-phenylselenohex-4-enyl)-2-methyl-2-vinyltetrahydrofuran

There total 3 articles about 5-(1,5-dimethyl-1-phenylselenohex-4-enyl)-2-methyl-2-vinyltetrahydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 80458-43-1
3,7,11-trimethyl-10-phenylselenododeca-1,6-diene-3,11-diol

: 80458-44-2,80458-46-4
3β-phenylselenocaparrapi oxide

: 82292-48-6
5-(1,5-dimethyl-1-phenylselenohex-4-enyl)-2-methyl-2-vinyltetrahydrofuran

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 0.0833333h;

Reference yield:

: 40716-66-3
(E)-3,7,11-trimethyl-1,6,10-dodecatrien-3-ol

: 82292-48-6
5-(1,5-dimethyl-1-phenylselenohex-4-enyl)-2-methyl-2-vinyltetrahydrofuran

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / aq.sodium hydrogen carbonate, m-chloroperbenzoic acid / CH₂Cl₂ / 20 h / Ambient temperature

2: 62 percent / 1.) sodium borohydride / ethanol / 1.) 0 deg C, 30 min, 2.) 14 h, room temperature

3: 48 percent / trifluoroacetic acid / CH₂Cl₂ / 0.08 h / 0 °C

With sodium tetrahydroborate; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In ethanol; dichloromethane;

Reference yield:

: 80458-42-0,131182-42-8,132435-55-3
(3RS)-10,11-epoxynerolidol

: 82292-48-6
5-(1,5-dimethyl-1-phenylselenohex-4-enyl)-2-methyl-2-vinyltetrahydrofuran

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / 1.) sodium borohydride / ethanol / 1.) 0 deg C, 30 min, 2.) 14 h, room temperature

2: 48 percent / trifluoroacetic acid / CH₂Cl₂ / 0.08 h / 0 °C

With sodium tetrahydroborate; trifluoroacetic acid; In ethanol; dichloromethane;