Dl-2-furylalanine

Base Information

• Chemical Name: Dl-2-furylalanine
• CAS No.: 4066-39-1
• Molecular Formula: C7H9NO3
• Molecular Weight: 155.153
• Hs Code.: 2932190090
• Mol file: 4066-39-1.mol

Synonyms:2-Furanpropanoicacid, a-amino-, (?à)-;2-Furanpropionic acid, a-amino-, DL- (8CI);2-Furanalanine;a-Amino-2-furanpropanoic acid;

Chemical Property of Dl-2-furylalanine

Chemical Property:

• Vapor Pressure: 0.001mmHg at 25°C
• Melting Point: 260oC
• Refractive Index: 1.541
• Boiling Point: 284.054 °C at 760 mmHg
• Flash Point: 125.591 °C
• PSA: 76.46000
• Density: 1.29 g/cm³
• LogP: 0.93430
• Storage Temp.: Keep in dark place,Inert atmosphere,Room temperature

Purity/Quality:

98%Min ^*data from raw suppliers

3-(2-Furyl)alanine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Dl-2-furylalanine

There total 15 articles about Dl-2-furylalanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

amino-furfuryl-malonic acid (4066-17-5) → (rac)-2-amino-3-furan-2-yl-propionic acid (4066-39-1)

Guidance literature:

With acetic acid; for 2.5h; Heating;

DOI:10.1248/cpb.45.1865

Reference yield: 77.0%

3-(furan-2-yl)-2-(hydroxyimino)propanoic acid (4066-14-2) → (rac)-2-amino-3-furan-2-yl-propionic acid (4066-39-1)

Guidance literature:

With formic acid; iron; zinc; at 60 - 65 ℃; for 2h;

DOI:10.1248/cpb.52.1137

Reference yield: 75.0%

(rac)-2-formylamino-3-furan-2-yl-propionic acid (4066-16-4) → (rac)-2-amino-3-furan-2-yl-propionic acid (4066-39-1)

Guidance literature:

With lithium hydroxide; at 60 ℃; for 2.5h;

DOI:10.1002/chem.200501034

upstream raw materials:

2-Chloromethylfuran

ethyl 2-acetamido-2-cyanoacetate

2-benzoylamino-3-furan-2-yl-propionic acid

amino-furfuryl-malonic acid

Downstream raw materials:

2-benzoylamino-3-furan-2-yl-propionic acid

2-(tert-butoxycarbonylamido)-3-(furan-2-yl)propanoic acid

(R)-2-amino-3-(2-furanyl)propionic acid

3-(fur-2-yl)crotonic acid