Benzyl(triphenyl)germane

Base Information

Chemical Name:Benzyl(triphenyl)germane
CAS No.:3246-98-8
Molecular Formula:C25H22Ge
Molecular Weight:395.04
Hs Code.:
NSC Number:170035
DSSTox Substance ID:DTXSID10305255
Nikkaji Number:J2.144.940G
Wikidata:Q82051832
Mol file:3246-98-8.mol

Synonyms:benzyl(triphenyl)germane;3246-98-8;NSC170035;DTXSID10305255;AKOS024433154;NSC-170035

Suppliers and Price of Benzyl(triphenyl)germane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 10 raw suppliers

Chemical Property of Benzyl(triphenyl)germane

Chemical Property:

Vapor Pressure:4.68E-09mmHg at 25°C
Boiling Point:484.1 °C at 760 mmHg
Flash Point:246.3 °C
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:5
Exact Mass:396.0933285
Heavy Atom Count:26
Complexity:347

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C[Ge](C2=CC=CC=C2)(C3=CC=CC=C3)C4=CC=CC=C4

Technology Process of Benzyl(triphenyl)germane

There total 8 articles about Benzyl(triphenyl)germane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 3839-32-5
triphenyl germyllithium

: 100-44-7
benzyl chloride

: 3246-98-8
triphenylbenzyl germanium

Guidance literature:: In tetrahydrofuran; at 0 - 20 ℃; for 1h;

Reference yield: 95.0%

: 105028-41-9
(α-phenylacetyl)triphenylgermane

: 3246-98-8
triphenylbenzyl germanium

Guidance literature:: In tetrahydrofuran; byproducts: CO; Irradiation (UV/VIS); irradn. a 400-W high pressure mercury lamp with stirring under argon for 30 min; removal of solvent with a rotary evaporator, purifn. by flash column chromatography, NMR, elem. anal.;
DOI:10.1246/bcsj.62.1361

Reference yield: 91.0%

: 1626-24-0
chlorotriphenylgermane

: 100-44-7
benzyl chloride

: 3246-98-8
triphenylbenzyl germanium

Guidance literature:: chlorotriphenylgermane; With naphthalene; lithium; In tetrahydrofuran; at 20 ℃; for 3h; Inert atmosphere;

benzyl chloride; In tetrahydrofuran; at 0 - 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/jacs.5b06587