(α-phenylacetyl)triphenylgermane

Base Information

Chemical Name:(α-phenylacetyl)triphenylgermane
CAS No.:105028-41-9
Molecular Formula:C₂₆H₂₂GeO
Molecular Weight:423.05
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (α-phenylacetyl)triphenylgermane

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Technology Process of (α-phenylacetyl)triphenylgermane

There total 1 articles about (α-phenylacetyl)triphenylgermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 3839-32-5
triphenylgermyl lithium

: 101-41-7
benzeneacetic acid methyl ester

: 105028-41-9
(α-phenylacetyl)triphenylgermane

Guidance literature:: In tetrahydrofuran; byproducts: LiOCH3, Ge(C6H5)3H; dropwise addn. of organic compd. (via syringe) to a soln. of Li-compd. (prepd. from GePh3 and BuLi in hexane) at room temp. under Ar, stirred for 10 min; quenched with aq. NH4Cl, organic layer extd. (ether), dried over MgSO4, evapd., flash chromy.;
DOI:10.1246/cl.1985.1829

Reference yield: 95.0%

: 105028-41-9
(α-phenylacetyl)triphenylgermane

: 3246-98-8
triphenylbenzyl germanium

Guidance literature:: In tetrahydrofuran; byproducts: CO; Irradiation (UV/VIS); irradn. a 400-W high pressure mercury lamp with stirring under argon for 30 min; removal of solvent with a rotary evaporator, purifn. by flash column chromatography, NMR, elem. anal.;
DOI:10.1246/bcsj.62.1361